phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

Base Information

Chemical Name:phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside
CAS No.:1448452-69-4
Molecular Formula:C₃₄H₄₈O₅SSi₂
Molecular Weight:624.989
Hs Code.:

Synonyms:phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

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Chemical Property of phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

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Technology Process of phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

There total 3 articles about phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1448452-70-7
phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-1-thio-α-L-arabinofuranoside

: 939-26-4
2-bromomethylnaphthyl bromide

: 1448452-69-4
phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c3ob40958a

Reference yield:

: 913060-77-2
phenyl 1-thio-α-L-arabinofuranoside

: 1448452-69-4
phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 °C / Inert atmosphere

With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3ob40958a

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 1448452-69-4
phenyl 3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-2-O-2-naphthylmethyl-1-thio-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 °C / Inert atmosphere

With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3ob40958a