4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione

Base Information

Chemical Name:4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione
CAS No.:74512-01-9
Molecular Formula:C₁₁H₉F₃N₂O₂S₃
Molecular Weight:354.398
Hs Code.:

Synonyms:4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione

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Chemical Property of 4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione

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Technology Process of 4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione

There total 3 articles about 4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 74512-00-8
tert-Butyl 2,4-dinitro-3-(n-propylamino)-6-(trifluoromethyl)phenyl trithiocarbonate

: 594-34-3
1,2-dibromo-2-methyl-propane

: 74512-01-9
4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione

Guidance literature:: With bromine; In chloroform; dimethyl sulfoxide; at 115 - 120 ℃; for 1h;
DOI:10.1021/jo01308a020

Reference yield: 40.0%

: 74512-00-8
tert-Butyl 2,4-dinitro-3-(n-propylamino)-6-(trifluoromethyl)phenyl trithiocarbonate

: 540-88-5
acetic acid tert-butyl ester

: 74512-01-9
4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione

Guidance literature:: With acetic acid; at 110 - 115 ℃; for 1.33333h;
DOI:10.1021/jo01308a020

Reference yield:

: 59431-93-5
2-Chloro-4-(n-propylamino)-3,5-dinitro(trifluoromethyl)benzene

: 74512-01-9
4-(n-propylamino)-5-nitro-7-(trifluoromethyl)-1,3-benzodithiole-2-thione

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / acetone / 1.) 5 deg C to 10 deg C; 2.) Room temperature, 2.5 h

2: 38 percent / glacial acetic acid / 1.33 h / 110 - 115 °C

With acetic acid; In acetone;
DOI:10.1021/jo01308a020