pent-4-enyl 2,3-di-O-benzyl-5-O-(2-O-benzyl-α-D-arabinofuranosyl)-α-D-arabinofuranoside

Base Information

Chemical Name:pent-4-enyl 2,3-di-O-benzyl-5-O-(2-O-benzyl-α-D-arabinofuranosyl)-α-D-arabinofuranoside
CAS No.:1431370-62-5
Molecular Formula:C₃₆H₄₄O₉
Molecular Weight:620.74
Hs Code.:

Synonyms:pent-4-enyl 2,3-di-O-benzyl-5-O-(2-O-benzyl-α-D-arabinofuranosyl)-α-D-arabinofuranoside

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Chemical Property of pent-4-enyl 2,3-di-O-benzyl-5-O-(2-O-benzyl-α-D-arabinofuranosyl)-α-D-arabinofuranoside

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Technology Process of pent-4-enyl 2,3-di-O-benzyl-5-O-(2-O-benzyl-α-D-arabinofuranosyl)-α-D-arabinofuranoside

There total 13 articles about pent-4-enyl 2,3-di-O-benzyl-5-O-(2-O-benzyl-α-D-arabinofuranosyl)-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431370-78-3
C₄₈H₇₀O₁₀Si₂

: 1431370-62-5
pent-4-enyl 2,3-di-O-benzyl-5-O-(2-O-benzyl-α-D-arabinofuranosyl)-α-D-arabinofuranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 25 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol400931p

Reference yield:

: 1431370-34-1
3,5-di-O-benzoyl-β-D-arabinofuranoside-prop-2-ynyl-1,2-orthobenzoate

: 1431370-62-5
pent-4-enyl 2,3-di-O-benzyl-5-O-(2-O-benzyl-α-D-arabinofuranosyl)-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 5 steps

1: gold(III) chloride / dichloromethane / 2 h / 25 °C / Molecular sieve; Inert atmosphere

2: sodium methylate / dichloromethane; methanol / 2 h / 25 °C / Inert atmosphere

3: pyridine / 2 h / 0 - 25 °C / Inert atmosphere

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 25 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 25 °C / Inert atmosphere

With pyridine; gold(III) chloride; tetrabutyl ammonium fluoride; sodium methylate; sodium hydride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol400931p

Reference yield:

: 1187620-69-4
pent-4-enyl 2,3-di-O-benzyl-α-D-arabinofuranoside

: 1431370-62-5
pent-4-enyl 2,3-di-O-benzyl-5-O-(2-O-benzyl-α-D-arabinofuranosyl)-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 5 steps

1: gold(III) chloride / dichloromethane / 2 h / 25 °C / Molecular sieve; Inert atmosphere

2: sodium methylate / dichloromethane; methanol / 2 h / 25 °C / Inert atmosphere

3: pyridine / 2 h / 0 - 25 °C / Inert atmosphere

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 25 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 25 °C / Inert atmosphere

With pyridine; gold(III) chloride; tetrabutyl ammonium fluoride; sodium methylate; sodium hydride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol400931p