dimethyl (R,S)-<1-2H>-2-phenyl-2-propenyl phosphite

Base Information

Chemical Name:dimethyl (R,S)-<1-2H>-2-phenyl-2-propenyl phosphite
CAS No.:151466-16-9
Molecular Formula:C₁₁H₁₅O₃P
Molecular Weight:227.204
Hs Code.:

Synonyms:dimethyl (R,S)-<1-2H>-2-phenyl-2-propenyl phosphite

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Chemical Property of dimethyl (R,S)-<1-2H>-2-phenyl-2-propenyl phosphite

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Technology Process of dimethyl (R,S)-<1-2H>-2-phenyl-2-propenyl phosphite

There total 3 articles about dimethyl (R,S)-<1-2H>-2-phenyl-2-propenyl phosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 20621-25-4
dimethoxy(diethylamino)phosphine

: 178817-64-6
[1-2H]-2-phenyl-2-propen-1-ol

: 151466-16-9
dimethyl (R,S)-<1-2H>-2-phenyl-2-propenyl phosphite

Guidance literature:: With 1H-tetrazole; In acetonitrile; for 10h; Ambient temperature;
DOI:10.1021/ja960428r

Reference yield:

: 4432-63-7
2-phenylacrolein

: 151466-16-9
dimethyl (R,S)-<1-2H>-2-phenyl-2-propenyl phosphite

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlD₄ / diethyl ether

2: 28 percent / 1H tetrazole / acetonitrile / 10 h / Ambient temperature

With 1H-tetrazole; lithium aluminium deuteride; In diethyl ether; acetonitrile;
DOI:10.1021/ja960428r

Reference yield:

: 6006-81-1
3-hydroxy-2-phenylpropene

: 151466-16-9
dimethyl (R,S)-<1-2H>-2-phenyl-2-propenyl phosphite

Guidance literature:: Multi-step reaction with 3 steps

1: MnO₂ / CH₂Cl₂ / 3 h / Ambient temperature

2: LiAlD₄ / diethyl ether

3: 28 percent / 1H tetrazole / acetonitrile / 10 h / Ambient temperature

With 1H-tetrazole; manganese(IV) oxide; lithium aluminium deuteride; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/ja960428r