2-chlorobenzoselenoamide

Base Information

• Chemical Name: 2-chlorobenzoselenoamide
• CAS No.: 156636-17-8
• Molecular Formula: C₇H₆ClNSe
• Molecular Weight: 218.544
• Mol file: 156636-17-8.mol

Synonyms:2-chlorobenzoselenoamide

Chemical Property of 2-chlorobenzoselenoamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-chlorobenzoselenoamide

There total 2 articles about 2-chlorobenzoselenoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-Chlorobenzonitrile (873-32-5) → 2-chlorobenzoselenoamide (156636-17-8)

Guidance literature:

2-Chlorobenzonitrile; With woollins’ reagent; In toluene; for 4h; Heating;

With water; In toluene; for 1h;

DOI:10.1021/ol062053c

Reference yield: 76.0%

2-Chlorobenzonitrile (873-32-5) + potassium 4-methylbenzenecarboselenoate → 2-chlorobenzoselenoamide (156636-17-8)

Guidance literature:

With boron trifluoride diethyl etherate; In tetrahydrofuran; at 0 ℃; for 5h;

DOI:10.1246/cl.1998.1287

Reference yield: 83.0%

2-chlorobenzoselenoamide (156636-17-8) → 3,5-bis(2-chlorophenyl)-1,2,4-selenadiazole

Guidance literature:

With thiourea; In acetonitrile; at 80 ℃; for 16h; Reagent/catalyst;

DOI:10.1016/j.tetlet.2018.01.063

upstream raw materials:

2-Chlorobenzonitrile