N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-1,3-phenylenediamine

Base Information

Chemical Name:N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-1,3-phenylenediamine
CAS No.:1373878-34-2
Molecular Formula:C₅₈H₇₀F₂N₂O₈
Molecular Weight:961.199
Hs Code.:

Synonyms:N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-1,3-phenylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-1,3-phenylenediamine

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Technology Process of N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-1,3-phenylenediamine

There total 4 articles about N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-1,3-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1363404-49-2
4-formyl-3-hydroxyphenyl 4-n-dodecyloxy-3-fluorobenzoate

: 108-45-2,64554-26-3,76583-20-5
m-phenylenediamine

: 1373878-34-2
N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-1,3-phenylenediamine

Guidance literature:: With acetic acid; In ethanol; at 20 ℃; for 24h;
DOI:10.3762/bjoc.8.15

Reference yield:

: 4-dodecyloxy-3-fluoro-benzoyl chloride

: 1373878-34-2
N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-1,3-phenylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / toluene / 16 h / 20 - 65 °C

2: acetic acid / ethanol / 24 h / 20 °C

With dmap; acetic acid; triethylamine; In ethanol; toluene;
DOI:10.3762/bjoc.8.15

Reference yield:

: 451-95-6
4-(dodecyloxy)-3-fluorobenzoic acid

: 1373878-34-2
N,N'-bis[4-(4-n-dodecyloxy-3-fluorobenzoyloxy)-2-hydroxybenzylidene]-1,3-phenylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; oxalyl dichloride / dichloromethane / 2 h / Reflux

2: dmap; triethylamine / toluene / 16 h / 20 - 65 °C

3: acetic acid / ethanol / 24 h / 20 °C

With pyridine; dmap; oxalyl dichloride; acetic acid; triethylamine; In ethanol; dichloromethane; toluene;
DOI:10.3762/bjoc.8.15