1-ethoxycarbonyl-3a,8-dimethyl-3-(4-nitrophenyl)-5-phenyl-3a,11-dihydro-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine

Base Information

• Chemical Name: 1-ethoxycarbonyl-3a,8-dimethyl-3-(4-nitrophenyl)-5-phenyl-3a,11-dihydro-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine
• CAS No.: 216696-56-9
• Molecular Formula: C₂₇H₂₅N₅O₄
• Molecular Weight: 483.527

Synonyms:1-ethoxycarbonyl-3a,8-dimethyl-3-(4-nitrophenyl)-5-phenyl-3a,11-dihydro-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine

Chemical Property of 1-ethoxycarbonyl-3a,8-dimethyl-3-(4-nitrophenyl)-5-phenyl-3a,11-dihydro-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine

Chemical Property:

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Technology Process of 1-ethoxycarbonyl-3a,8-dimethyl-3-(4-nitrophenyl)-5-phenyl-3a,11-dihydro-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine

There total 1 articles about 1-ethoxycarbonyl-3a,8-dimethyl-3-(4-nitrophenyl)-5-phenyl-3a,11-dihydro-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.2%

C10H10N2O2BrNO2 (20147-56-2) + 1,5-benzodiazepine → 1-ethoxycarbonyl-3a,8-dimethyl-3-(4-nitrophenyl)-5-phenyl-3a,11-dihydro-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine (216696-56-9)

Guidance literature:

With triethylamine; In benzene; at 20 ℃; for 40h;

DOI:10.1080/00397919809458689

Reference yield: 56.0%

N-(p-methyl)-phenyl-C-acetylformohydrazidoyl bromide (58670-19-2) + 1-ethoxycarbonyl-3a,8-dimethyl-3-(4-nitrophenyl)-5-phenyl-3a,11-dihydro-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine (216696-56-9) → 1,7-diethoxycarbonyl-3a,10-dimethyl-3-(4-nitrophenyl)-5-(4-toyly)-3a,4a,8,13-tetrahydro-4H-bis[1,2,4-triazolo][4,3-a:3',4'-d][1,5]benzodiazepine + 1,7-diethoxycarbonyl-3a,10-dimethyl-3-(4-nitrophenyl)-5-(4-toyly)-3a,4a,8,13-tetrahydro-4H-bis[1,2,4-triazolo][4,3-a:3',4'-d][1,5]benzodiazepine

Guidance literature:

With triethylamine; In benzene; at 20 ℃; for 40h; Title compound not separated from byproducts;

DOI:10.1080/00397919809458689

Reference yield: 41.0%

C10H10BrClN2O2 + 1-ethoxycarbonyl-3a,8-dimethyl-3-(4-nitrophenyl)-5-phenyl-3a,11-dihydro-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine (216696-56-9) → 5-(4-chlorophenyl)-1,7-diethoxycarbonyl-3a,10-dimethyl-3-(4-nitrophenyl)-3a,4a,8,13-tetrahydro-4H-bis[1,2,4-triazolo][4,3-a:3',4'-d][1,5]benzodiazepine + 5-(4-chlorophenyl)-1,7-diethoxycarbonyl-3a,10-dimethyl-3-(4-nitrophenyl)-3a,4a,8,13-tetrahydro-4H-bis[1,2,4-triazolo][4,3-a:3',4'-d][1,5]benzodiazepine

Guidance literature:

With triethylamine; In benzene; at 20 ℃; for 40h;

DOI:10.1080/00397919809458689

upstream raw materials:

C₁₀H₁₀N₂O₂BrNO₂

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