3-(4-bromobenzyl)-1-(3,5-dichlorophenyl)-5,6-diiodo-3-methyl-1H-imidazo[1,2-α]imidazol-2-one

Base Information

• Chemical Name: 3-(4-bromobenzyl)-1-(3,5-dichlorophenyl)-5,6-diiodo-3-methyl-1H-imidazo[1,2-α]imidazol-2-one
• CAS No.: 321724-15-6
• Molecular Formula: C₁₉H₁₂BrCl₂I₂N₃O
• Molecular Weight: 702.943

Synonyms:3-(4-bromobenzyl)-1-(3,5-dichlorophenyl)-5,6-diiodo-3-methyl-1H-imidazo[1,2-α]imidazol-2-one

Chemical Property of 3-(4-bromobenzyl)-1-(3,5-dichlorophenyl)-5,6-diiodo-3-methyl-1H-imidazo[1,2-α]imidazol-2-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 3-(4-bromobenzyl)-1-(3,5-dichlorophenyl)-5,6-diiodo-3-methyl-1H-imidazo[1,2-α]imidazol-2-one

There total 5 articles about 3-(4-bromobenzyl)-1-(3,5-dichlorophenyl)-5,6-diiodo-3-methyl-1H-imidazo[1,2-α]imidazol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

3-(4-bromo-benzyl)-1-(3,5-dichloro-phenyl)-3-methyl-1H-imidazo[1,2-a]imidazol-2-one (321723-65-3) → 3-(4-bromobenzyl)-1-(3,5-dichlorophenyl)-5,6-diiodo-3-methyl-1H-imidazo[1,2-α]imidazol-2-one (321724-15-6)

Guidance literature:

With N-iodo-succinimide; pyridinium p-toluenesulfonate; In dichloromethane; at 0 ℃;

DOI:10.1021/jm049657b

Reference yield:

3,5-dichlorophenylisothiocyanate (6590-93-8) → 3-(4-bromobenzyl)-1-(3,5-dichlorophenyl)-5,6-diiodo-3-methyl-1H-imidazo[1,2-α]imidazol-2-one (321724-15-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 90 percent / dioxane / 90 °C

2: 1.96 g / toluene / 130 - 140 °C

3: trifluoroacetic acid / CH₂Cl₂ / 90 °C

4: 60 percent / N-iodosuccinimide; pyridinium p-toluenesulfonate / CH₂Cl₂ / 0 °C

With N-iodo-succinimide; pyridinium p-toluenesulfonate; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; toluene;

DOI:10.1021/jm049657b

Reference yield:

ethyl 2-amino-2-(4-bromobenzyl)-propanoate (213202-98-3) → 3-(4-bromobenzyl)-1-(3,5-dichlorophenyl)-5,6-diiodo-3-methyl-1H-imidazo[1,2-α]imidazol-2-one (321724-15-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 90 percent / dioxane / 90 °C

2: 1.96 g / toluene / 130 - 140 °C

3: trifluoroacetic acid / CH₂Cl₂ / 90 °C

4: 60 percent / N-iodosuccinimide; pyridinium p-toluenesulfonate / CH₂Cl₂ / 0 °C

With N-iodo-succinimide; pyridinium p-toluenesulfonate; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; toluene;

DOI:10.1021/jm049657b

upstream raw materials:

3-(4-bromo-benzyl)-1-(3,5-dichloro-phenyl)-3-methyl-1H-imidazo[1,2-a]imidazol-2-one

3,5-dichlorophenylisothiocyanate

ethyl 2-amino-2-(4-bromobenzyl)-propanoate

5-(4-bromobenzyl)-3-(3,5-dichlorophenyl)-5-methyl-2-thioxoimidazolidin-4-one

Downstream raw materials:

3-(4-bromo-benzyl)-1-(3,5-dichloro-phenyl)-6-iodo-3-methyl-1H-imidazo[1,2-a]imidazol-2-one

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