Technology Process of C39H42N2O6Si
There total 9 articles about C39H42N2O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C46H56N2O9Si;
With
hydrogenchloride;
In
1,4-dioxane; dichloromethane;
for 1.5h;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
toluene;
at 110 ℃;
for 0.583333h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: Dess-Martin periodane / dichloromethane / 18 h / 20 °C / Cooling with ice
2.1: sodium tetrahydroborate / methanol / 0.5 h / 0 - 20 °C
3.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h
4.1: lithium borohydride / tetrahydrofuran / 18 h / 20 °C / Cooling with ice
5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice
6.1: hydrazine hydrate / ethanol / 2 h / 70 °C
7.1: sodium hydrogencarbonate / ethanol; water / 20 h
8.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1.5 h
8.2: 0.58 h / 110 °C
With
1H-imidazole; hydrogenchloride; sodium tetrahydroborate; lithium borohydride; di-isopropyl azodicarboxylate; sodium hydrogencarbonate; Dess-Martin periodane; hydrazine hydrate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 - 20 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h
3.1: lithium borohydride / tetrahydrofuran / 18 h / 20 °C / Cooling with ice
4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice
5.1: hydrazine hydrate / ethanol / 2 h / 70 °C
6.1: sodium hydrogencarbonate / ethanol; water / 20 h
7.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1.5 h
7.2: 0.58 h / 110 °C
With
1H-imidazole; hydrogenchloride; sodium tetrahydroborate; lithium borohydride; di-isopropyl azodicarboxylate; sodium hydrogencarbonate; hydrazine hydrate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;