5-(1,3-dihydroxy-4,4,5,5-tetramethyl-imidazolidin-2-yl)-isophthalic acid

Base Information

Chemical Name:5-(1,3-dihydroxy-4,4,5,5-tetramethyl-imidazolidin-2-yl)-isophthalic acid
CAS No.:226249-81-6
Molecular Formula:C₁₅H₂₀N₂O₆
Molecular Weight:324.334
Hs Code.:

Synonyms:5-(1,3-dihydroxy-4,4,5,5-tetramethyl-imidazolidin-2-yl)-isophthalic acid

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Chemical Property of 5-(1,3-dihydroxy-4,4,5,5-tetramethyl-imidazolidin-2-yl)-isophthalic acid

Chemical Property:

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Technology Process of 5-(1,3-dihydroxy-4,4,5,5-tetramethyl-imidazolidin-2-yl)-isophthalic acid

There total 6 articles about 5-(1,3-dihydroxy-4,4,5,5-tetramethyl-imidazolidin-2-yl)-isophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 14538-51-3,78375-92-5
2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate

: 66998-60-5
5-formyl-1,3-benzene dicarboxylic acid

: 226249-81-6
5-(1,3-dihydroxy-4,4,5,5-tetramethyl-imidazolidin-2-yl)-isophthalic acid

Guidance literature:: DOI:10.1016/S0040-4039(99)00330-5

Reference yield:

: 4105-93-5
1,3-bis(ethoxycarbonyl)benzoic acid

: 226249-81-6
5-(1,3-dihydroxy-4,4,5,5-tetramethyl-imidazolidin-2-yl)-isophthalic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 86 percent / Me₂S-BH₃ / tetrahydrofuran

2: 85 percent / MnO₂ / CH₂Cl₂

3: 86 percent / para-toluenesulfonic acid / toluene

4: 86 percent / NaOH / aq. ethanol

5: HCl / acetone

6: 67 percent

With hydrogenchloride; manganese(IV) oxide; sodium hydroxide; dimethylsulfide borane complex; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; dichloromethane; acetone; toluene;
DOI:10.1016/S0040-4039(99)00330-5

Reference yield:

: 181425-91-2
diethyl 5-(hydroxymethyl)isophthalate

: 226249-81-6
5-(1,3-dihydroxy-4,4,5,5-tetramethyl-imidazolidin-2-yl)-isophthalic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / MnO₂ / CH₂Cl₂

2: 86 percent / para-toluenesulfonic acid / toluene

3: 86 percent / NaOH / aq. ethanol

4: HCl / acetone

5: 67 percent

With hydrogenchloride; manganese(IV) oxide; sodium hydroxide; toluene-4-sulfonic acid; In ethanol; dichloromethane; acetone; toluene;
DOI:10.1016/S0040-4039(99)00330-5