C₆₃H₉₆ClIO₁₁Si₂

Base Information

Chemical Name:C₆₃H₉₆ClIO₁₁Si₂
CAS No.:868381-34-4
Molecular Formula:C₆₃H₉₆ClIO₁₁Si₂
Molecular Weight:1247.98
Hs Code.:

C<sub>63</sub>H<sub>96</sub>ClIO<sub>11</sub>Si<sub>2</sub>

Synonyms:C₆₃H₉₆ClIO₁₁Si₂

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Chemical Property of C₆₃H₉₆ClIO₁₁Si₂

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Technology Process of C₆₃H₉₆ClIO₁₁Si₂

There total 36 articles about C₆₃H₉₆ClIO₁₁Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 392692-68-1
C₆₃H₉₆Cl₂O₁₁Si₂

: 868381-34-4
C₆₃H₉₆ClIO₁₁Si₂

Guidance literature:: With sodium hydrogencarbonate; 1-iodo-propane; sodium iodide; sodium sulfite; In acetone; for 18h;
DOI:10.1055/s-2005-871960

Reference yield:

: 847053-68-3
2,4-dichloro-pent-4-enoic acid ethyl ester

: 868381-34-4
C₆₃H₉₆ClIO₁₁Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: DBU / benzene / 4 h / 0 - 20 °C

2: DIBAL-H / CH₂Cl₂ / 0.5 h / -78 °C

3: 81 percent / MnO₂ / CH₂Cl₂ / 1 h / 20 °C

4: diethyl ether / 16 h / -78 °C

5: imidazole / dimethylformamide / 2 h / 20 °C

6: 75 percent / Zn; PbI₂; Me₃SiCl / TiCl₄ / CH₂Cl₂; tetrahydrofuran / 4 h / 20 °C

7: 93 percent / NaI; n-PrI; NaHCO₃ / Na₂SO₃ / acetone / 18 h

With 1H-imidazole; manganese(IV) oxide; chloro-trimethyl-silane; diisobutylaluminium hydride; sodium hydrogencarbonate; 1-iodo-propane; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; lead(II) iodide; zinc; titanium tetrachloride; sodium sulfite; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1055/s-2005-871960

Reference yield:

: (2R,3S,4R,5R,6S)-2-Hydroxymethyl-5-methyl-6-(2-methyl-[1,3]dioxolan-2-ylmethyl)-tetrahydro-pyran-3,4-diol

: 868381-34-4
C₆₃H₉₆ClIO₁₁Si₂

Guidance literature:: Multi-step reaction with 22 steps

1.1: imidazole / dimethylformamide / 3 h / 20 °C

2.1: 98 percent / NaI; NaH / tetrahydrofuran; dimethylformamide / 18 h / 20 °C

3.1: 88 percent / TBAF / tetrahydrofuran / 2 h / 20 °C

4.1: 100 percent / I₂; PPh₃; imidazole / acetonitrile; diethyl ether

5.1: 92 percent / 18-crown-6 / dimethylformamide / 3 h / 20 °C

6.1: DIBAL-H / CH₂Cl₂ / 2 h / -78 °C

7.1: aq. NaClO₂; 2-methyl-2-butene / 2-methyl-propan-2-ol; tetrahydrofuran; various solvent(s) / 1 h / 20 °C / pH 7

8.1: TEA; EDCI; HOBt / CH₂Cl₂

9.1: 90 percent / aq. PPTS / acetone / 1 h / Heating

10.1: t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran / 0.33 h / -78 °C

10.2: 100 percent / 2-methyl-propan-2-ol; tetrahydrofuran / 1 h / -78 °C

11.1: aq. H₂O₂; pyridine; methyltrioxorhenium / CH₂Cl₂ / 4 h / 0 - 20 °C

11.2: 78 percent / TBAF / CH₂Cl₂ / 0.5 h / 0 °C

12.1: BF₃*OEt₂ / CH₂Cl₂ / 20 °C

13.1: TEA / diethyl ether / 1.5 h / 0 °C

14.1: 3 h / -78 - 0 °C

15.1: 89 percent / PPTS; TMOF / tetrahydrofuran / 0.33 h / 20 °C

16.1: 86 percent / 2,6-lutidine / tetrahydrofuran / 0.33 h / -78 °C

17.1: 96 percent / CeCl₃ / tetrahydrofuran / 0.33 h / -78 °C

18.1: TEA / diethyl ether / 3 h / -78 °C

19.1: diethyl ether / 16 h / -78 °C

20.1: imidazole / dimethylformamide / 2 h / 20 °C

21.1: 75 percent / Zn; PbI₂; Me₃SiCl / TiCl₄ / CH₂Cl₂; tetrahydrofuran / 4 h / 20 °C

22.1: 93 percent / NaI; n-PrI; NaHCO₃ / Na₂SO₃ / acetone / 18 h

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; sodium chlorite; chloro-trimethyl-silane; cerium(III) chloride; 2-methyl-but-2-ene; 18-crown-6 ether; TEA; boron trifluoride diethyl etherate; potassium tert-butylate; tetrabutyl ammonium fluoride; dihydrogen peroxide; iodine; pyridinium p-toluenesulfonate; methyltrioxorhenium(VII); sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; benzotriazol-1-ol; 1-iodo-propane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; sodium iodide; lead(II) iodide; zinc; trimethyl orthoformate; titanium tetrachloride; sodium sulfite; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.1055/s-2005-871960