11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocycloheptapyridazino<4,5-a>cycl<3.3.2>azine

Base Information

Chemical Name:11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocycloheptapyridazino<4,5-a>cycl<3.3.2>azine
CAS No.:102408-92-4
Molecular Formula:C₂₉H₂₃N₃
Molecular Weight:413.522
Hs Code.:

11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocyclohepta<ef>pyridazino<4,5-a>cycl<3.3.2>azine

Synonyms:11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocycloheptapyridazino<4,5-a>cycl<3.3.2>azine

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Chemical Property of 11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocycloheptapyridazino<4,5-a>cycl<3.3.2>azine

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Technology Process of 11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocycloheptapyridazino<4,5-a>cycl<3.3.2>azine

There total 3 articles about 11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocycloheptapyridazino<4,5-a>cycl<3.3.2>azine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 102408-87-7
1,2-dibenzoyl-3-methyl-4,5,6,7-tetrahydrocycloheptacycl<3.3.2>azine

: 102408-92-4
11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocycloheptapyridazino<4,5-a>cycl<3.3.2>azine

Guidance literature:: With hydrogenchloride; hydrazine hydrate; In ethanol; for 1h; Heating;
DOI:10.1002/jhet.5570220425

Reference yield:

: 7197-96-8
2,3-cycloheptenopyridine

: 102408-92-4
11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocycloheptapyridazino<4,5-a>cycl<3.3.2>azine

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / acetone / 1) 2 h, reflux; 2) room temp., overnight

2: 2) DDQ / 1) THF, 0 deg C; 2) t < 0 deg C, 10 min.

3: 95 percent / hydrazine hydrate, conc. HCl / ethanol / 1 h / Heating

With hydrogenchloride; hydrazine hydrate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In ethanol; acetone;
DOI:10.1002/jhet.5570220425

Reference yield:

: 102408-77-5
N-acetonyl-2,3-cycloheptenopyridinium bromide

: 102408-92-4
11-methyl-1,4-diphenyl-7,8,9,10-tetrahydrocycloheptapyridazino<4,5-a>cycl<3.3.2>azine

Guidance literature:: Multi-step reaction with 2 steps

1: 2) DDQ / 1) THF, 0 deg C; 2) t < 0 deg C, 10 min.

2: 95 percent / hydrazine hydrate, conc. HCl / ethanol / 1 h / Heating

With hydrogenchloride; hydrazine hydrate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In ethanol;
DOI:10.1002/jhet.5570220425