Technology Process of C27H38N8O4
There total 5 articles about C27H38N8O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C30H42N8O4;
With
trifluoroacetic acid;
In
trifluoroacetic acid;
at 20 ℃;
for 1h;
In
methanol;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
2.1: 2-iodoxybenzoic acid / ethyl acetate / 2 h / Reflux
3.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
4.1: trifluoroacetic acid / trifluoroacetic acid / 1 h / 20 °C
4.2: basic resin / 0.5 h / 20 °C
With
2-iodoxybenzoic acid; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; ethyl acetate; 1,2-dichloro-ethane; trifluoroacetic acid;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
2.1: 2-iodoxybenzoic acid / ethyl acetate / 2 h / Reflux
3.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
4.1: trifluoroacetic acid / trifluoroacetic acid / 1 h / 20 °C
4.2: basic resin / 0.5 h / 20 °C
With
2-iodoxybenzoic acid; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; ethyl acetate; 1,2-dichloro-ethane; trifluoroacetic acid;