C₃₃H₂₇ClN₂O₄

Base Information

Chemical Name:C₃₃H₂₇ClN₂O₄
CAS No.:1423684-54-1
Molecular Formula:C₃₃H₂₇ClN₂O₄
Molecular Weight:551.041
Hs Code.:

C<sub>33</sub>H<sub>27</sub>ClN<sub>2</sub>O<sub>4</sub>

Synonyms:C₃₃H₂₇ClN₂O₄

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Chemical Property of C₃₃H₂₇ClN₂O₄

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Technology Process of C₃₃H₂₇ClN₂O₄

There total 17 articles about C₃₃H₂₇ClN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1423701-52-3
C₃₄H₂₉ClN₂O₄

: 1423684-54-1
C₃₃H₂₇ClN₂O₄

Guidance literature:: C₃₄H₂₉ClN₂O₄; With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; at 20 ℃;

With hydrogenchloride; In water; pH=3;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1423684-54-1
C₃₃H₂₇ClN₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / dimethyl sulfoxide / 20 °C

2.1: acetic acid; iron / ethanol / 100 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

4.1: water; sodium hydroxide / methanol; tetrahydrofuran / 20 h / 80 °C

5.1: diphenyl phosphoryl azide; triethylamine / toluene / 2 h / Reflux

6.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 2 h / Reflux; Inert atmosphere

7.1: hydrogenchloride / methanol / 4 h / 40 °C

8.1: methanol; potassium carbonate / 0.17 h / 0 - 20 °C

9.1: water; lithium hydroxide monohydrate / methanol; tetrahydrofuran / 20 °C

9.2: pH 3

With hydrogenchloride; methanol; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium hydroxide monohydrate; diphenyl phosphoryl azide; water; iron; sodium hydride; sodium carbonate; potassium carbonate; acetic acid; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 1423684-54-1
C₃₃H₂₇ClN₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C

2.1: diphenyl phosphoryl azide; triethylamine / toluene / 2 h / Reflux

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 2 h / Reflux; Inert atmosphere

4.1: hydrogenchloride / methanol / 4 h / 40 °C

5.1: methanol; potassium carbonate / 0.17 h / 0 - 20 °C

6.1: water; lithium hydroxide monohydrate / methanol; tetrahydrofuran / 20 °C

6.2: pH 3

With hydrogenchloride; methanol; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium hydroxide monohydrate; dimethylsulfide borane complex; diphenyl phosphoryl azide; water; sodium carbonate; potassium carbonate; triethylamine; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; toluene;