(1R,2R,3R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-cyclohex-4-ene-1,2-dicarboxylic acid dimethyl ester

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Chemical Name:(1R,2R,3R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-cyclohex-4-ene-1,2-dicarboxylic acid dimethyl ester
CAS No.:250696-26-5
Molecular Formula:C₃₂H₄₃NO₅Si
Molecular Weight:549.783
Hs Code.:

Synonyms:(1R,2R,3R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-cyclohex-4-ene-1,2-dicarboxylic acid dimethyl ester

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Chemical Property of (1R,2R,3R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-cyclohex-4-ene-1,2-dicarboxylic acid dimethyl ester

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Technology Process of (1R,2R,3R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-cyclohex-4-ene-1,2-dicarboxylic acid dimethyl ester

There total 1 articles about (1R,2R,3R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-cyclohex-4-ene-1,2-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 624-48-6
dimethyl cis-but-2-ene-1,4-dioate

: 192460-78-9
1-[2,5-(R,R)-diphenyl-pyrrolidin-1-yl]-3-(tert-butyldimethylsiloxy)-1,3-butadiene

: 250696-26-5
(1R,2R,3R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-cyclohex-4-ene-1,2-dicarboxylic acid dimethyl ester

Guidance literature:: In toluene; at 20 ℃;
DOI:10.1021/ja971272d

Reference yield:

: 250696-26-5
(1R,2R,3R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-cyclohex-4-ene-1,2-dicarboxylic acid dimethyl ester

: [(1R,2S,6R)-4-(tert-Butyl-dimethyl-silanyloxy)-2-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-6-hydroxymethyl-cyclohex-3-enyl]-methanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -78 ℃; for 3h;
DOI:10.1021/ja9921930

Reference yield:

: 250696-26-5
(1R,2R,3R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((2R,5R)-2,5-diphenyl-pyrrolidin-1-yl)-cyclohex-4-ene-1,2-dicarboxylic acid dimethyl ester

: (4R,5R)-4,5-bis(hydroxymethyl)-cyclohex-2-ene-1-one

Guidance literature:: With lithium aluminium tetrahydride; hydrogen fluoride; Multistep reaction; 1) Et2O, -78 deg C -> room temperature, 2) CH3CN, H2O, room temperature, 1 h;
DOI:10.1021/ja971272d