1-dimethyl-tert-butylsilyloxy-2-(5-methyl-2H-tetrazol-2-yl)-3-trityloxypropane

Base Information

Chemical Name:1-dimethyl-tert-butylsilyloxy-2-(5-methyl-2H-tetrazol-2-yl)-3-trityloxypropane
CAS No.:140711-51-9
Molecular Formula:C₃₀H₃₈N₄O₂Si
Molecular Weight:514.743
Hs Code.:

Synonyms:1-dimethyl-tert-butylsilyloxy-2-(5-methyl-2H-tetrazol-2-yl)-3-trityloxypropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-dimethyl-tert-butylsilyloxy-2-(5-methyl-2H-tetrazol-2-yl)-3-trityloxypropane

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Technology Process of 1-dimethyl-tert-butylsilyloxy-2-(5-methyl-2H-tetrazol-2-yl)-3-trityloxypropane

There total 3 articles about 1-dimethyl-tert-butylsilyloxy-2-(5-methyl-2H-tetrazol-2-yl)-3-trityloxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 126272-25-1
1-dimethyl-tert-butylsilyloxy-3-trityloxypropan-2-ol

: 4076-36-2
5-methyltetrazole

: 140711-51-9
1-dimethyl-tert-butylsilyloxy-2-(5-methyl-2H-tetrazol-2-yl)-3-trityloxypropane

: 140711-50-8
1-dimethyl-tert-butylsilyloxy-2-(5-methyl-1H-tetrazol-1-yl)-3-trityloxypropane

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; Ambient temperature;
DOI:10.1248/cpb.40.85

Reference yield:

: 16975-62-5,17327-05-8,118014-34-9,18325-46-7
tritylglycerol

: 140711-51-9
1-dimethyl-tert-butylsilyloxy-2-(5-methyl-2H-tetrazol-2-yl)-3-trityloxypropane

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide

2: 64 percent / PPh₃, diethyl azodicarboxylate (DEAD) / tetrahydrofuran / Ambient temperature

With 1H-imidazole; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1248/cpb.40.85

Reference yield:

: 76-83-5
trityl chloride

: 140711-51-9
1-dimethyl-tert-butylsilyloxy-2-(5-methyl-2H-tetrazol-2-yl)-3-trityloxypropane

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂

2: imidazole / dimethylformamide

3: 64 percent / PPh₃, diethyl azodicarboxylate (DEAD) / tetrahydrofuran / Ambient temperature

With 1H-imidazole; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.40.85