C₂₃H₃₆O₄Si

Base Information

Chemical Name:C₂₃H₃₆O₄Si
CAS No.:1195988-14-7
Molecular Formula:C₂₃H₃₆O₄Si
Molecular Weight:404.622
Hs Code.:

C<sub>23</sub>H<sub>36</sub>O<sub>4</sub>Si

Synonyms:C₂₃H₃₆O₄Si

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Chemical Property of C₂₃H₃₆O₄Si

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Technology Process of C₂₃H₃₆O₄Si

There total 1 articles about C₂₃H₃₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₃₀O₃Si

: 16139-79-0
ethyl diphenylphosphonoacetate

: 1195988-14-7
C₂₃H₃₆O₄Si

Guidance literature:: ethyl diphenylphosphonoacetate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

C₁₉H₃₀O₃Si; In tetrahydrofuran; mineral oil; at -78 - 40 ℃; for 10h;
DOI:10.1016/j.tet.2010.11.017

Reference yield:

: 1195988-14-7
C₂₃H₃₆O₄Si

: 1195988-26-1
C₂₁H₃₄O₃Si

Guidance literature:: C₂₃H₃₆O₄Si; With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 - -50 ℃; for 0.5h;

With methanol; Rochelle's salt; In hexane; dichloromethane; water; at -78 - 20 ℃;
DOI:10.1016/j.tet.2010.11.017

Reference yield:

: 1195988-14-7
C₂₃H₃₆O₄Si

: 1195988-16-9
C₁₅H₂₀O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 - -50 °C

1.2: -78 - 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 13 h / 0 - 20 °C

3.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide / dichloromethane / 9 h / -40 - -25 °C / Molecular sieve

3.2: 1.5 h / -25 - 20 °C

With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; dichloromethane; 3.1: Sharpless epoxidation;
DOI:10.1016/j.tet.2010.11.017