5′(S)-C-(benzyloxymethyl)-2′,3′-di-O-(tert-butyldimethylsilyl)-uridine

Base Information

Chemical Name:5′(S)-C-(benzyloxymethyl)-2′,3′-di-O-(tert-butyldimethylsilyl)-uridine
CAS No.:1620571-34-7
Molecular Formula:C₂₉H₄₈N₂O₇Si₂
Molecular Weight:592.88
Hs Code.:

Synonyms:5′(S)-C-(benzyloxymethyl)-2′,3′-di-O-(tert-butyldimethylsilyl)-uridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5′(S)-C-(benzyloxymethyl)-2′,3′-di-O-(tert-butyldimethylsilyl)-uridine

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Technology Process of 5′(S)-C-(benzyloxymethyl)-2′,3′-di-O-(tert-butyldimethylsilyl)-uridine

There total 2 articles about 5′(S)-C-(benzyloxymethyl)-2′,3′-di-O-(tert-butyldimethylsilyl)-uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1620571-25-6
5′(S)-C-(butylaminomethyl)-2′,3′-di-O-(tert-butyldimethylsilyl)uridine

: 100-51-6,185532-71-2
benzyl alcohol

: 1620571-34-7
5′(S)-C-(benzyloxymethyl)-2′,3′-di-O-(tert-butyldimethylsilyl)-uridine

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 60 ℃; for 16h; regioselective reaction;
DOI:10.1021/jo501410m

Reference yield:

: 1620571-24-5
C₂₂H₄₀N₂O₅Si₂

: 1620571-34-7
5′(S)-C-(benzyloxymethyl)-2′,3′-di-O-(tert-butyldimethylsilyl)-uridine

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 30 °C

2: sodium hydride / tetrahydrofuran; mineral oil / 16 h / 0 - 60 °C

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/jo501410m