{(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside

Base Information

Chemical Name:{(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside
CAS No.:1026073-86-8
Molecular Formula:C₇₈H₈₆O₁₆
Molecular Weight:1279.53
Hs Code.:

{(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside

Synonyms:{(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside

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Chemical Property of {(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside

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Technology Process of {(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside

There total 1 articles about {(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1026073-85-7
(1R,2R,3S)-3-ethyl-2-(((2S,3S,4R,5R,6S)-3,4,5-tris(benzyloxy)-6-methyltetrahydro-2H-pyran-2-yl)oxy)cyclohexan-1-ol

: 322761-81-9
ethyl 3-O-[(1S)-1-(cyclohexylmethyl)-2-oxo-2-(phenylmethoxy)ethyl]-1-thio-β-D-galactopyranoside 2,4,6-tribenzoate

: 1026073-86-8
{(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside

Guidance literature:: (1R,2R,3S)-3-ethyl-2-(((2S,3S,4R,5R,6S)-3,4,5-tris(benzyloxy)-6-methyltetrahydro-2H-pyran-2-yl)oxy)cyclohexan-1-ol; ethyl 3-O-[(1S)-1-(cyclohexylmethyl)-2-oxo-2-(phenylmethoxy)ethyl]-1-thio-β-D-galactopyranoside 2,4,6-tribenzoate; In dichloromethane; at 20 ℃; for 4h; Molecular sieve;

With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; for 49.5h; Molecular sieve;

Reference yield: 77.0%

: 1026073-86-8
{(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside

: 1026232-61-0
{(1R,2R,3S)-2-[(6-deoxy-α-L-galactopyranosyl)oxy]-3-ethyl-cyclohex-1-yl}2-O-benzoyl-3-O-[(1S)-1-carboxy-2-cyclohexyl-ethyl]-β-D-galactopyranoside

Guidance literature:: {(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside; With hydrogen; palladium hydroxide on carbon; In 1,4-dioxane; water; at 20 ℃; for 24h; under 3620.13 Torr;

With methanol; sodium methylate; at 20 ℃; for 16h;

With acetic acid; In methanol;

Reference yield:

: 1026073-86-8
{(1R,2R,3S)-2-[(2,3,4-tri-O-benzyl-6-deoxy-α-L-galactopyranosyl)oxy]-3-ethylcyclohex-1-yl} 2,4,6-tri-O-benzoyl-3-O-[(1S)-1-benzyloxycarbonyl-2-cyclohexylethyl]-β-D-galactopyranoside

: C₅₇H₆₈O₁₆

Guidance literature:: With 10% Pd(OH)₂ on C; hydrogen; In 1,4-dioxane; water; at 20 ℃; for 72h; under 3750.38 Torr;
DOI:10.1002/chem.201102884