3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-4-{[4-(10-undecen-1-yloxy)benzoyl]oxy}-1,1'-biphenyl

Base Information

Chemical Name:3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-4-{[4-(10-undecen-1-yloxy)benzoyl]oxy}-1,1'-biphenyl
CAS No.:887947-25-3
Molecular Formula:C₅₄H₅₃F₉O₈
Molecular Weight:1001
Hs Code.:

Synonyms:3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-4-{[4-(10-undecen-1-yloxy)benzoyl]oxy}-1,1'-biphenyl

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Chemical Property of 3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-4-{[4-(10-undecen-1-yloxy)benzoyl]oxy}-1,1'-biphenyl

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Technology Process of 3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-4-{[4-(10-undecen-1-yloxy)benzoyl]oxy}-1,1'-biphenyl

There total 4 articles about 3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-4-{[4-(10-undecen-1-yloxy)benzoyl]oxy}-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-1,1'-biphenyl-4-ol

: 59100-95-7
4-(10-undecenyloxy)benzoic acid

: 887947-25-3
3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-4-{[4-(10-undecen-1-yloxy)benzoyl]oxy}-1,1'-biphenyl

Guidance literature:: With dmap; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1002/anie.200503402

Reference yield:

: 809285-98-1
4'-(benzyloxy)-1,1'-biphenyl-3-ol

: 887947-25-3
3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-4-{[4-(10-undecen-1-yloxy)benzoyl]oxy}-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / N-Cy-N'-[2-(N-methylmorpholinium)ethyl]carbodiimide tosylate; DMAP / CH₂Cl₂ / 48 h / 20 °C

2: 90 percent / hydrogen / Pd/C / ethyl acetate / 24 h / 3040 Torr

3: 78 percent / N-Cy-N'-[2-(N-methylmorpholinium)ethyl]carbodiimide tosylate; DMAP / CH₂Cl₂ / 48 h / 20 °C

With dmap; hydrogen; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1002/anie.200503402

Reference yield:

: 260056-65-3
4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoic acid

: 887947-25-3
3'-{[4-({4-[(7,7,8,8,9,9,10,10,10-nonafluorodecyl)oxy]benzoyl}oxy)benzoyl]oxy}-4-{[4-(10-undecen-1-yloxy)benzoyl]oxy}-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / N-Cy-N'-[2-(N-methylmorpholinium)ethyl]carbodiimide tosylate; DMAP / CH₂Cl₂ / 48 h / 20 °C

2: 90 percent / hydrogen / Pd/C / ethyl acetate / 24 h / 3040 Torr

3: 78 percent / N-Cy-N'-[2-(N-methylmorpholinium)ethyl]carbodiimide tosylate; DMAP / CH₂Cl₂ / 48 h / 20 °C

With dmap; hydrogen; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1002/anie.200503402