N-{[(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)cyclopentyl]aminocarbonyl}-3-methoxy-2-propenamide

Base Information

Chemical Name:N-{[(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)cyclopentyl]aminocarbonyl}-3-methoxy-2-propenamide
CAS No.:405095-83-2
Molecular Formula:C₁₈H₃₀N₂O₆
Molecular Weight:370.446
Hs Code.:

Synonyms:N-{[(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)cyclopentyl]aminocarbonyl}-3-methoxy-2-propenamide

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Chemical Property of N-{[(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)cyclopentyl]aminocarbonyl}-3-methoxy-2-propenamide

Chemical Property:

Purity/Quality:

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Hazard Codes:

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Useful:

Technology Process of N-{[(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)cyclopentyl]aminocarbonyl}-3-methoxy-2-propenamide

There total 1 articles about N-{[(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)cyclopentyl]aminocarbonyl}-3-methoxy-2-propenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 174230-82-1
β-methoxyacryloyl isocyanate

: 405095-82-1
(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)-1-cyclopentanamine

: 405095-83-2
N-{[(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)cyclopentyl]aminocarbonyl}-3-methoxy-2-propenamide

Guidance literature:: In N,N-dimethyl-formamide; at -20 - 20 ℃; for 12.25h;

Reference yield:

: 405095-83-2
N-{[(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)cyclopentyl]aminocarbonyl}-3-methoxy-2-propenamide

: 71184-20-8
D-(-)-carbodine

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonia; water / 1,4-dioxane; ethanol / 20 h / 100 °C / Steel bomb

2.1: dmap; 2,4,6-triisopropylphenylsulfonyl chloride; triethylamine / acetonitrile / 12 h / 20 °C

2.2: 5 h

3.1: trifluoroacetic acid / water / 4 h / 70 °C

With dmap; 2,4,6-triisopropylphenylsulfonyl chloride; ammonia; water; triethylamine; trifluoroacetic acid; In 1,4-dioxane; ethanol; water; acetonitrile;

Reference yield:

: 405095-83-2
N-{[(1R,2S,3R,4R)-4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)cyclopentyl]aminocarbonyl}-3-methoxy-2-propenamide

: 1070967-50-8
(1R,2S,3R,4R)-1-[4-(tert-butoxymethyl)-2,3-(isopropylidenedioxy)-cyclopentan-1-yl]-cytosine

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonia; water / 1,4-dioxane; ethanol / 20 h / 100 °C / Steel bomb

2.1: dmap; 2,4,6-triisopropylphenylsulfonyl chloride; triethylamine / acetonitrile / 12 h / 20 °C

2.2: 5 h

With dmap; 2,4,6-triisopropylphenylsulfonyl chloride; ammonia; water; triethylamine; In 1,4-dioxane; ethanol; acetonitrile;