methyl (E)-3-(N₆-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)prop-2-enoate

Base Information

• Chemical Name: methyl (E)-3-(N₆-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)prop-2-enoate
• CAS No.: 1182207-15-3
• Molecular Formula: C₂₃H₂₅N₅O₆
• Molecular Weight: 467.481

Synonyms:methyl (E)-3-(N₆-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)prop-2-enoate

Chemical Property of methyl (E)-3-(N₆-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)prop-2-enoate

Chemical Property:

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Technology Process of methyl (E)-3-(N₆-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)prop-2-enoate

There total 1 articles about methyl (E)-3-(N₆-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tert-butyl N6-[(benzyloxy)carbonyl]-8-formyladenine-9-acetate (1182207-14-2) + methyl (triphenylphosphoranylidene)acetate (21204-67-1,2605-67-6) → methyl (E)-3-(N6-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)prop-2-enoate (1182207-15-3)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1002/hlca.200900047

Reference yield: 73.0%

methyl (E)-3-(N6-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)prop-2-enoate (1182207-15-3) → methyl 3-(N6-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)propanoate (1182207-16-4)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 ℃; Inert atmosphere;

DOI:10.1002/hlca.200900047

upstream raw materials:

tert-butyl N₆-[(benzyloxy)carbonyl]-8-formyladenine-9-acetate

methyl (triphenylphosphoranylidene)acetate

Downstream raw materials:

methyl 3-(N₆-[(benzyloxy)carbonyl]-9-{[(tert-butoxy)carbonyl]methyl}adenine-8-yl)propanoate

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