Technology Process of C32H41N7O5
There total 5 articles about C32H41N7O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C38H55N7O5Si;
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
With
water;
In
tetrahydrofuran;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetonitrile / 12 h / 90 °C
2.1: triethylamine / dmap / dichloromethane / 18 h / 5 - 20 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C
3.2: Cooling with ice
With
tetrabutyl ammonium fluoride; potassium carbonate; triethylamine;
dmap;
In
tetrahydrofuran; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium phosphate / tris-(dibenzylideneacetone)dipalladium(0); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane; water / 15 h / 80 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 10 °C
2.2: 1 h / 20 °C / Inert atmosphere
3.1: potassium carbonate / acetonitrile / 12 h / 90 °C
4.1: triethylamine / dmap / dichloromethane / 18 h / 5 - 20 °C / Inert atmosphere
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C
5.2: Cooling with ice
With
potassium phosphate; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; triethylamine;
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dmap; tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
