C₁₄H₁₅N₃O₃S

Base Information

Chemical Name:C₁₄H₁₅N₃O₃S
CAS No.:1425495-13-1
Molecular Formula:C₁₄H₁₅N₃O₃S
Molecular Weight:305.357
Hs Code.:

C<sub>14</sub>H<sub>15</sub>N<sub>3</sub>O<sub>3</sub>S

Synonyms:C₁₄H₁₅N₃O₃S

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Chemical Property of C₁₄H₁₅N₃O₃S

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Technology Process of C₁₄H₁₅N₃O₃S

There total 10 articles about C₁₄H₁₅N₃O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1425495-12-0
C₁₅H₁₈O₆S₂

: 1425495-13-1
C₁₄H₁₅N₃O₃S

: C₁₄H₁₅N₃O₃S

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 2h;
DOI:10.1002/ejoc.201200906

Reference yield:

: 89-67-8
α-D-glucoheptonic γ-lactone

: 1425495-13-1
C₁₄H₁₅N₃O₃S

: C₁₄H₁₅N₃O₃S

Guidance literature:: Multi-step reaction with 9 steps

1: hydrogen bromide; acetic acid / 1 h

2: perchloric acid / 1 h

3: sodium sulfite; sodium disulfite / methanol; water / 3.5 h / 20 °C

4: hydrogenchloride / methanol / 72 h / 20 °C

5: silver(l) oxide / toluene / 1 h / 80 °C / Inert atmosphere

6: silver(l) oxide / toluene / 3.5 h / 80 °C

7: benzyltriethylammonium tetrathiomolybdate / acetonitrile; ethanol / 5 h / 20 °C

8: pyridine / 3 h / 0 - 20 °C

9: sodium azide / N,N-dimethyl-formamide / 2 h / 80 °C

With pyridine; hydrogenchloride; sodium disulfite; sodium azide; perchloric acid; benzyltriethylammonium tetrathiomolybdate; hydrogen bromide; acetic acid; silver(l) oxide; sodium sulfite; In methanol; ethanol; water; N,N-dimethyl-formamide; toluene; acetonitrile; 7: |Michael Addition;
DOI:10.1002/ejoc.201200906

Reference yield:

: 116386-12-0
2,7-dibromo-2,7-dideoxy-D-glycero-D-ido-heptono-1,4-lactone

: 1425495-13-1
C₁₄H₁₅N₃O₃S

: C₁₄H₁₅N₃O₃S

Guidance literature:: Multi-step reaction with 8 steps

1: perchloric acid / 1 h

2: sodium sulfite; sodium disulfite / methanol; water / 3.5 h / 20 °C

3: hydrogenchloride / methanol / 72 h / 20 °C

4: silver(l) oxide / toluene / 1 h / 80 °C / Inert atmosphere

5: silver(l) oxide / toluene / 3.5 h / 80 °C

6: benzyltriethylammonium tetrathiomolybdate / acetonitrile; ethanol / 5 h / 20 °C

7: pyridine / 3 h / 0 - 20 °C

8: sodium azide / N,N-dimethyl-formamide / 2 h / 80 °C

With pyridine; hydrogenchloride; sodium disulfite; sodium azide; perchloric acid; benzyltriethylammonium tetrathiomolybdate; silver(l) oxide; sodium sulfite; In methanol; ethanol; water; N,N-dimethyl-formamide; toluene; acetonitrile; 6: |Michael Addition;
DOI:10.1002/ejoc.201200906