3S-(-)-1,1-dimethylethyl 3-aminocarbonyl-4-<<<(4-nitro-2,6-dichlorophenyl)amino>carbonyl>methyl>-1-piperazinecarboxylate

Base Information

Chemical Name:3S-(-)-1,1-dimethylethyl 3-aminocarbonyl-4-<<<(4-nitro-2,6-dichlorophenyl)amino>carbonyl>methyl>-1-piperazinecarboxylate
CAS No.:166520-14-5
Molecular Formula:C₁₈H₂₃Cl₂N₅O₆
Molecular Weight:476.317
Hs Code.:

Synonyms:3S-(-)-1,1-dimethylethyl 3-aminocarbonyl-4-<<<(4-nitro-2,6-dichlorophenyl)amino>carbonyl>methyl>-1-piperazinecarboxylate

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Chemical Property of 3S-(-)-1,1-dimethylethyl 3-aminocarbonyl-4-<<<(4-nitro-2,6-dichlorophenyl)amino>carbonyl>methyl>-1-piperazinecarboxylate

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Technology Process of 3S-(-)-1,1-dimethylethyl 3-aminocarbonyl-4-<<<(4-nitro-2,6-dichlorophenyl)amino>carbonyl>methyl>-1-piperazinecarboxylate

There total 6 articles about 3S-(-)-1,1-dimethylethyl 3-aminocarbonyl-4-<<<(4-nitro-2,6-dichlorophenyl)amino>carbonyl>methyl>-1-piperazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112257-24-6
tert-butyl 3-(aminocarbonyl)piperazine-1-carboxylate

: 166520-14-5
3S-(-)-1,1-dimethylethyl 3-aminocarbonyl-4-<<<(4-nitro-2,6-dichlorophenyl)amino>carbonyl>methyl>-1-piperazinecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: Tris buffer pH 8.2 / 168 h / Ambient temperature; L-leucine aminopeptidase

2: NH₃ / methanol / 72 h / 0 °C

3: methanol / 1 h / Ambient temperature

4: Et₃N / dimethylformamide / 1.5 h

With Tris buffer pH 8.2; ammonia; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1080/00397919508011814

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 166520-14-5
3S-(-)-1,1-dimethylethyl 3-aminocarbonyl-4-<<<(4-nitro-2,6-dichlorophenyl)amino>carbonyl>methyl>-1-piperazinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 1 h / Ambient temperature

2: Et₃N / dimethylformamide / 1.5 h

With triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1080/00397919508011814

Reference yield:

: 159572-93-7
(S)-(-)-Piperazine-2-carboxamide

: 166520-14-5
3S-(-)-1,1-dimethylethyl 3-aminocarbonyl-4-<<<(4-nitro-2,6-dichlorophenyl)amino>carbonyl>methyl>-1-piperazinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 1 h / Ambient temperature

2: Et₃N / dimethylformamide / 1.5 h

With triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1080/00397919508011814