5-(2-benzoyloxy-ethyl)-3-benzyl-2-(diethoxyphosphoryloxy-phenyl-methyl)-4-methyl-thiazolium; bromide

Base Information

• Chemical Name: 5-(2-benzoyloxy-ethyl)-3-benzyl-2-(diethoxyphosphoryloxy-phenyl-methyl)-4-methyl-thiazolium; bromide
• CAS No.: 17511-95-4
• Molecular Formula: Br*C₃₁H₃₅NO₆PS
• Molecular Weight: 660.566

Synonyms:5-(2-benzoyloxy-ethyl)-3-benzyl-2-(diethoxyphosphoryloxy-phenyl-methyl)-4-methyl-thiazolium; bromide

Chemical Property of 5-(2-benzoyloxy-ethyl)-3-benzyl-2-(diethoxyphosphoryloxy-phenyl-methyl)-4-methyl-thiazolium; bromide

Chemical Property:

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Technology Process of 5-(2-benzoyloxy-ethyl)-3-benzyl-2-(diethoxyphosphoryloxy-phenyl-methyl)-4-methyl-thiazolium; bromide

There total 1 articles about 5-(2-benzoyloxy-ethyl)-3-benzyl-2-(diethoxyphosphoryloxy-phenyl-methyl)-4-methyl-thiazolium; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl benzoylphosphonate (3277-27-8) + 5-(2-benzoyloxy-ethyl)-3-benzyl-4-methyl-thiazolium; bromide → 5-(2-benzoyloxy-ethyl)-3-benzyl-2-(diethoxyphosphoryloxy-phenyl-methyl)-4-methyl-thiazolium; bromide (17511-95-4)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide;

DOI:10.1021/jo01275a009

Reference yield:

5-(2-benzoyloxy-ethyl)-3-benzyl-2-(diethoxyphosphoryloxy-phenyl-methyl)-4-methyl-thiazolium; bromide (17511-95-4) → 1-benzoyloxy-2-(3-benzyl-2-benzylidene-4-methyl-2,3-dihydro-thiazol-5-yl)-ethane (17528-36-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/jo01275a009

Reference yield:

5-(2-benzoyloxy-ethyl)-3-benzyl-2-(diethoxyphosphoryloxy-phenyl-methyl)-4-methyl-thiazolium; bromide (17511-95-4) → 5-(2-benzoyloxy-ethyl)-3-benzyl-4-methyl-3H-thiazol-2-one (20962-91-8)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd-C / methanol

2: O₃ / CHCl₃

With hydrogen; ozone; palladium on activated charcoal; In methanol; chloroform;

DOI:10.1021/jo01275a009

upstream raw materials:

diethyl benzoylphosphonate

Downstream raw materials:

2-(4-benzyl-5-methyl-3-oxo-2-phenyl-2,3-dihydro-4H-1,4-thiazin-6-yl)ethyl benzoate

1-benzoyloxy-2-(3-benzyl-2-benzylidene-4-methyl-2,3-dihydro-thiazol-5-yl)-ethane

1-benzoyloxy-2-(4-benzyl-5-dimethylamino-3-methyl-6-phenyl-4H-[1,4]thiazin-2-yl)-ethane

1-benzoyloxy-2-(4-benzyl-3-methyl-5-methylimino-6-phenyl-5,6-dihydro-4H-[1,4]thiazin-2-yl)-ethane

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