N^α-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol

Base Information

Chemical Name:N^α-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol
CAS No.:220237-32-1
Molecular Formula:C₃₁H₃₇NO₇
Molecular Weight:535.637
Hs Code.:

N<sup>α</sup>-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol

Synonyms:N^α-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol

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Technology Process of N^α-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol

There total 5 articles about N^α-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: (4-bromomethyl)-phenoxy-allyl acetate

: 220237-31-0
N^α-(Dde)-L-tyrosinol

: 220237-32-1
N^α-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol

Guidance literature:: With caesium carbonate; In acetonitrile; for 3h; Heating;
DOI:10.1021/jo981546v

Reference yield:

: 1755-15-3
2-acetyldimedone

: 220237-32-1
N^α-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / Et₃N / dimethylformamide / overnight

2: 98 percent / CF₃COOH / CH₂Cl₂ / 0.67 h / Ambient temperature

3: 89 percent / Cs₂CO₃ / acetonitrile / 3 h / Heating

With caesium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo981546v

Reference yield:

: 187526-99-4
(9H-fluoren-9-yl)methyl (S)-(1-(4-(tert-butoxy)phenyl)-3-hydroxypropan-2-yl)carbamate

: 220237-32-1
N^α-(Dde)-O-(4-methylphenoxy-allyl acetate)-L-tyrosinol

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / Et₂NH / CH₂Cl₂ / 3 h

2: 90 percent / Et₃N / dimethylformamide / overnight

3: 98 percent / CF₃COOH / CH₂Cl₂ / 0.67 h / Ambient temperature

4: 89 percent / Cs₂CO₃ / acetonitrile / 3 h / Heating

With caesium carbonate; diethylamine; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo981546v