α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid ethyl ester

Base Information

Chemical Name:α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid ethyl ester
CAS No.:167014-56-4
Molecular Formula:C₂₃H₂₉NO₃
Molecular Weight:367.488
Hs Code.:

Synonyms:α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid ethyl ester

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Chemical Property of α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid ethyl ester

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Technology Process of α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid ethyl ester

There total 1 articles about α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28178-42-9
2,6-diisopropylphenyl isocyanate

: 101-97-3
Ethyl 2-phenylethanoate

: 167014-56-4
α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid ethyl ester

Guidance literature:: With lithium diisopropyl amide; Multistep reaction; 1.) THF, -78 deg C, 2 min, 2.) THF, -78 deg C, 1.5 h;
DOI:10.1021/jm9604033

Reference yield: 82.0%

: 167014-56-4
α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid ethyl ester

: 167014-57-5
α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm970560h

Reference yield:

: 167014-56-4
α-[[[2,6-bis(1-methylethyl)phenyl]amino]carbonyl]benzene acetic acid ethyl ester

: N-(2,6-Diisopropyl-phenyl)-2-phenyl-malonamic acid 1,1-dimethyl-pentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / aq. NaOH / tetrahydrofuran / Ambient temperature

2: DCC / CH₂Cl₂ / 0 - 20 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm970560h