(2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester

Base Information

Chemical Name:(2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester
CAS No.:212970-63-3
Molecular Formula:C₃₀H₄₉NO₆
Molecular Weight:519.722
Hs Code.:

Synonyms:(2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester

Suppliers and Price of (2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester

There total 10 articles about (2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 212970-62-2
(4E,9Z)-6-Oxo-trideca-4,9-dienal

: 212970-55-3
(2Z,6E,11E)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester

: 212970-63-3
(2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester

Guidance literature:: With piperidine; acetic acid; In dichloromethane; at -20 ℃; for 48h;
DOI:10.1016/S0040-4039(98)01196-4

Reference yield:

: 31502-21-3
(E)-oct-4-en-1-ol

: 212970-63-3
(2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / PCC/Al₂O₃ / tetrahydrofuran

2: 86 percent / tetrahydrofuran / -78 °C

3: 90 percent / LAH / tetrahydrofuran / 65 °C

4: 82 percent / Dess-Martin periodinane

5: 67 percent / piperidinium acetate / CH₂Cl₂ / 72 h / -20 °C

6: piperidine, HOAc / CH₂Cl₂ / 48 h / -20 °C

With piperidine; aluminum oxide; lithium aluminium tetrahydride; piperdinium acetate; Dess-Martin periodane; acetic acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(98)01196-4

Reference yield:

: 78693-35-3
4E-octenal

: 212970-63-3
(2Z,6E,11Z)-2-Hexanoyl-8-oxo-pentadeca-2,6,11-trienoic acid 4-tert-butoxycarbonylamino-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / tetrahydrofuran / -78 °C

2: 90 percent / LAH / tetrahydrofuran / 65 °C

3: 82 percent / Dess-Martin periodinane

4: 67 percent / piperidinium acetate / CH₂Cl₂ / 72 h / -20 °C

5: piperidine, HOAc / CH₂Cl₂ / 48 h / -20 °C

With piperidine; lithium aluminium tetrahydride; piperdinium acetate; Dess-Martin periodane; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(98)01196-4