(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid

Base Information

Chemical Name:(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid
CAS No.:89637-89-8
Molecular Formula:C₇H₈O₃S*C₂₉H₄₀N₄O₇
Molecular Weight:728.864
Hs Code.:

(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid

Synonyms:(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid

Suppliers and Price of (S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid

There total 3 articles about (S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 27317-68-6
Boc-Lys(Z)-Lys(Z)-OMe

: 104-15-4
toluene-4-sulfonic acid

: 89637-89-8
(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: In benzene; for 1h; Heating;
DOI:10.1021/jm00373a014

Reference yield:

: 2389-45-9
Boc-Lys(Z)-OH

: 89637-89-8
(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / Et₃N, diphenylphosphoryl azide / dimethylformamide / 0 - 20 °C

2: 90 percent / benzene / 1 h / Heating

With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00373a014

Reference yield:

: 27894-50-4
methyl (2S)-2-amino-6-{[(benzyloxy)carbonyl]amino}hexanoate hydrochloride

: 89637-89-8
(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / Et₃N, diphenylphosphoryl azide / dimethylformamide / 0 - 20 °C

2: 90 percent / benzene / 1 h / Heating

With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00373a014