6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose

Base Information

Chemical Name:6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose
CAS No.:148324-13-4
Molecular Formula:C₁₇H₂₄O₇S
Molecular Weight:372.439
Hs Code.:

Synonyms:6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose

Suppliers and Price of 6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose

There total 2 articles about 6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 94844-70-9
5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 148324-13-4
6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose

Guidance literature:: With trifluorormethanesulfonic acid; In diethyl ether; 1.) 0 deg C, 5 min, 2.) RT, 17 h;
DOI:10.1248/cpb.41.282

Reference yield:

: 74152-53-7
O¹,O²-isopropylidene-O³-methanesulfonyl-α-D-xylo-5,6-dideoxy-hex-5-enofuranose

: 148324-13-4
6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-O-methanesulfonyl-D-glucofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) borane methylsulfide complex, 2.) 15 percent NaOH, H₂O₂ / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 2 h

2: 100 percent / trifluoromethanesulfonic acid (TfOH) / diethyl ether / 1.) 0 deg C, 5 min, 2.) RT, 17 h

With sodium hydroxide; borane methylsulfide; trifluorormethanesulfonic acid; dihydrogen peroxide; In diethyl ether;
DOI:10.1248/cpb.41.282