1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate

Base Information

Chemical Name:1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate
CAS No.:1202761-36-1
Molecular Formula:C₂HF₃O₂*C₁₅H₂₀N₂O₄
Molecular Weight:406.359
Hs Code.:

Synonyms:1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate

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Chemical Property of 1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate

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Technology Process of 1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate

There total 1 articles about 1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 926904-07-6
1-benzyl-4-tert-butyl-2-ethyl (S)-piperazine-1,2,4-tricarboxylate

: 1202761-36-1
1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2.166h;

Reference yield: 81.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1202761-36-1
1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate

: 926904-08-7
1-benzyl-2-ethyl (S)-4-methyl-piperazine-1,2-dicarboxylate

Guidance literature:: formaldehyd; 1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate; With sodium acetate; In tetrahydrofuran; at 20 ℃; for 2h; Molecular sieve;

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; at 0 - 20 ℃; for 68.5h;

Reference yield: 55.0%

: 1445-73-4
1-Methyl-4-piperidone

: 1202761-36-1
1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate

: 926904-15-6
1-benzyl-2-ethyl (S)-4-(1-methyl-piperidin-4-yl)-piperazine-1,2-dicarboxylate

Guidance literature:: 1-Methyl-4-piperidone; 1-benzyl-2-ethyl (S)-piperazine-1,2-dicarboxylate trifluoroacetate; In tetrahydrofuran; at 20 ℃; for 1h;

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; at 0 - 20 ℃;