2,6-diethyl-4-methyl-N-(5,6,7-trihydroquinolin-8-ylidene)phenylamine

Base Information

• Chemical Name: 2,6-diethyl-4-methyl-N-(5,6,7-trihydroquinolin-8-ylidene)phenylamine
• CAS No.: 1263563-78-5
• Molecular Formula: C₂₀H₂₄N₂
• Molecular Weight: 292.424
• Mol file: 1263563-78-5.mol

Synonyms:2,6-diethyl-4-methyl-N-(5,6,7-trihydroquinolin-8-ylidene)phenylamine

Chemical Property of 2,6-diethyl-4-methyl-N-(5,6,7-trihydroquinolin-8-ylidene)phenylamine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2,6-diethyl-4-methyl-N-(5,6,7-trihydroquinolin-8-ylidene)phenylamine

There total 1 articles about 2,6-diethyl-4-methyl-N-(5,6,7-trihydroquinolin-8-ylidene)phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,6,7,8-tetrahydro-8-quinolinone (56826-69-8) + 2,6-diethyl-4-methylaniline (24544-08-9) → N-(2,6-diethyl-4-methylphenyl)-5,6-dihydroquinolin-8-amine + 2,6-diethyl-4-methyl-N-(5,6,7-trihydroquinolin-8-ylidene)phenylamine (1263563-78-5)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; Reflux; Inert atmosphere;

DOI:10.1039/c1dt10541h

Reference yield: 89.0%

dichloro bis(acetonitrile) palladium(II) (21264-30-2,90243-59-7,14592-56-4) + 2,6-diethyl-4-methyl-N-(5,6,7-trihydroquinolin-8-ylidene)phenylamine (1263563-78-5) → N-(5,6,7-trihydroquinolin-8-ylidene)-2,6-diethyl-4-methylphenyliminopalladium(II) dichloride

Guidance literature:

In dichloromethane; at 20 ℃; Inert atmosphere; Schlenk technique;

DOI:10.3390/molecules21121686

Reference yield: 84.0%

chloromethyl(1,5-cyclooctadiene)palladium(II) + 2,6-diethyl-4-methyl-N-(5,6,7-trihydroquinolin-8-ylidene)phenylamine (1263563-78-5) → C21H27ClN2Pd

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1039/c6nj04019e

upstream raw materials:

5,6,7,8-tetrahydro-8-quinolinone

2,6-diethyl-4-methylaniline