1,2-<(carbonylamino)carbonyl>-1β-(3,4-dichlorophenyl)-6α-hydroxy-N-methyl-4-cyclohexenyl acetate

Base Information

• Chemical Name: 1,2-<(carbonylamino)carbonyl>-1β-(3,4-dichlorophenyl)-6α-hydroxy-N-methyl-4-cyclohexenyl acetate
• CAS No.: 79735-26-5
• Molecular Formula: C₁₇H₁₅Cl₂NO₄
• Molecular Weight: 368.216

Synonyms:1,2-<(carbonylamino)carbonyl>-1β-(3,4-dichlorophenyl)-6α-hydroxy-N-methyl-4-cyclohexenyl acetate

Chemical Property of 1,2-<(carbonylamino)carbonyl>-1β-(3,4-dichlorophenyl)-6α-hydroxy-N-methyl-4-cyclohexenyl acetate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2-<(carbonylamino)carbonyl>-1β-(3,4-dichlorophenyl)-6α-hydroxy-N-methyl-4-cyclohexenyl acetate

There total 3 articles about 1,2-<(carbonylamino)carbonyl>-1β-(3,4-dichlorophenyl)-6α-hydroxy-N-methyl-4-cyclohexenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.4%

1-acetoxy-1,3-butadiene (1515-76-0) + N-methyl-2-(3,4-dichlorophenyl)maleimide (79722-40-0) → 1,2-<(carbonylamino)carbonyl>-1β-(3,4-dichlorophenyl)-6α-hydroxy-N-methyl-4-cyclohexenyl acetate (79735-26-5)

Guidance literature:

With hydroquinone; In chloroform; for 72h; Heating;

DOI:10.1021/jo00341a034

Reference yield:

N-methylmaleimide (930-88-1) → 1,2-<(carbonylamino)carbonyl>-1β-(3,4-dichlorophenyl)-6α-hydroxy-N-methyl-4-cyclohexenyl acetate (79735-26-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) HNO₂/CuCl₂ / 2.) lutidine

2: 74.4 percent / hydroquinone / CHCl₃ / 72 h / Heating

With cis-nitrous acid; hydroquinone; copper dichloride; In chloroform;

DOI:10.1021/jo00341a034

Reference yield:

m,p-dichloroaniline (95-76-1) → 1,2-<(carbonylamino)carbonyl>-1β-(3,4-dichlorophenyl)-6α-hydroxy-N-methyl-4-cyclohexenyl acetate (79735-26-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) HNO₂/CuCl₂ / 2.) lutidine

2: 74.4 percent / hydroquinone / CHCl₃ / 72 h / Heating

With cis-nitrous acid; hydroquinone; copper dichloride; In chloroform;

DOI:10.1021/jo00341a034

upstream raw materials:

1-acetoxy-1,3-butadiene

N-methyl-2-(3,4-dichlorophenyl)maleimide

N-methylmaleimide

m,p-dichloroaniline

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