phenyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:phenyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside
CAS No.:904691-44-7
Molecular Formula:C₆₇H₅₄O₁₇S
Molecular Weight:1163.22
Hs Code.:

Synonyms:phenyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

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Technology Process of phenyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

There total 3 articles about phenyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: C₃₇H₃₁Cl₂NO₁₀

: 150935-65-2
phenyl 2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

: 904691-44-7
phenyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

Guidance literature:: C₃₇H₃₁Cl₂NO₁₀; phenyl 2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside; In dichloromethane; at 0 ℃; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/acs.joc.1c00250

Reference yield: 72.0%

: 105376-04-3,113214-71-4,138661-53-7
ethyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-galactopyranoside

: 150935-65-2
phenyl 2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

: 904691-44-7
phenyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 2-((trifluoromethyl)thio)benzo[d]isothiazol-3(2H)-one 1,1-dioxide; In dichloromethane; at -30 - 20 ℃; for 0.5h; stereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.201900265

Reference yield: 70.0%

: 150935-65-2
phenyl 2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

: 203435-09-0
2,3,4,6-tetra-O-benzoyl-α,b-D-galactopyranosyl trichloroacetimidate

: 904691-44-7
phenyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

Guidance literature:: With molecular sieve; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 0.5h;
DOI:10.1002/anie.200600591