(2S,3R)-2-Benzyloxycarbonylamino-3-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylmethoxy)-butyric acid benzyl ester

Base Information

Chemical Name:(2S,3R)-2-Benzyloxycarbonylamino-3-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylmethoxy)-butyric acid benzyl ester
CAS No.:669089-96-7
Molecular Formula:C₃₄H₄₁NO₁₄
Molecular Weight:687.698
Hs Code.:

Synonyms:(2S,3R)-2-Benzyloxycarbonylamino-3-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylmethoxy)-butyric acid benzyl ester

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Chemical Property of (2S,3R)-2-Benzyloxycarbonylamino-3-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylmethoxy)-butyric acid benzyl ester

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Technology Process of (2S,3R)-2-Benzyloxycarbonylamino-3-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylmethoxy)-butyric acid benzyl ester

There total 3 articles about (2S,3R)-2-Benzyloxycarbonylamino-3-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylmethoxy)-butyric acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 86122-64-7
benzyl (2S,3S)-1-benzyloxycarbonyl-3-methyl-aziridine-2-carboxylate

: 497880-75-8
1,3,4,5-tetra-O-acetyl-2,6-anhydro-D-glycero-L-galacto-heptitol

: 669089-96-7
(2S,3R)-2-Benzyloxycarbonylamino-3-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylmethoxy)-butyric acid benzyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In chloroform; at 20 ℃; for 32h;
DOI:10.1016/j.bmcl.2003.10.011

Reference yield:

: Acetic acid (2R,3S,4S,5R,6S)-3,5-diacetoxy-2-acetoxymethyl-6-formyl-tetrahydro-pyran-4-yl ester

: 669089-96-7
(2S,3R)-2-Benzyloxycarbonylamino-3-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylmethoxy)-butyric acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NaBH₄ / tetrahydrofuran

2: 55 percent / BF₃*Et₂O / CHCl₃ / 32 h / 20 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; In tetrahydrofuran; chloroform;
DOI:10.1016/j.bmcl.2003.10.011

Reference yield:

: 4163-60-4
β-D-galactose peracetate

: 669089-96-7
(2S,3R)-2-Benzyloxycarbonylamino-3-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-ylmethoxy)-butyric acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 48 percent / BF₃*Et₂O / acetonitrile

2: O₃ / CH₂Cl₂

3: 62 percent / NaBH₄ / tetrahydrofuran

4: 55 percent / BF₃*Et₂O / CHCl₃ / 32 h / 20 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; ozone; In tetrahydrofuran; dichloromethane; chloroform; acetonitrile;
DOI:10.1016/j.bmcl.2003.10.011