(1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide

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Chemical Name:(1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide
CAS No.:1313358-21-2
Molecular Formula:C₄₀H₅₂N₆O₅
Molecular Weight:696.89
Hs Code.:

(1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide

Synonyms:(1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide

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Chemical Property of (1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide

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Technology Process of (1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide

There total 5 articles about (1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 198904-87-9
(2S,3S)-3-amino-4-phenyl-1-(1-(4-(pyridin-2-yl)benzyl)hydrazinyl)butan-2-ol hydrochloride

: 308287-83-4
(1S,3R)-(+)-3-(2-Acetamido)-2,2-dimethylcyclobutanecarboxylic acid

: 1313358-21-2
(1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide

Guidance literature:: (1S,3R)-(+)-3-(2-Acetamido)-2,2-dimethylcyclobutanecarboxylic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; at 0 ℃;

(2S,3S)-3-amino-4-phenyl-1-(1-(4-(pyridin-2-yl)benzyl)hydrazinyl)butan-2-ol hydrochloride; With 4-methyl-morpholine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 80-57-9,1196-01-6
(-)-Verbenone

: 1313358-21-2
(1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium periodate; water / ruthenium(III) trichloride hydrate / tetrachloromethane; acetonitrile / 12 h / 0 - 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

3.1: sodium azide; methanesulfonic acid / 1,2-dimethoxyethane / 48 h / -45 - 20 °C

4.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1 h / 20 °C

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0 °C

5.2: 16 h / 20 °C

With sodium periodate; sodium azide; methanesulfonic acid; water; hydrogen; caesium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; ruthenium(III) trichloride hydrate; palladium 10% on activated carbon; In tetrachloromethane; 1,2-dimethoxyethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 3.1: Schmidt Reaction;

Reference yield:

: 288848-24-8
(1S,3R)-3-acetyl-2,2-dimethylcyclobutane carboxylic acid

: 1313358-21-2
(1S,3R)-3-acetamido-N-((2S,3S)-4-(2-((1S,3R)-3-acetamido-2,2-dimethylcyclobutanecarbonyl)-1-(4-(pyridin-2-yl)benzyl)hydrazinyl)-3-hydroxy-1-phenylbutan-2-yl)-2,2-dimethylcyclobutanecarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

2.1: sodium azide; methanesulfonic acid / 1,2-dimethoxyethane / 48 h / -45 - 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1 h / 20 °C

4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0 °C

4.2: 16 h / 20 °C

With sodium azide; methanesulfonic acid; hydrogen; caesium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; palladium 10% on activated carbon; In 1,2-dimethoxyethane; ethyl acetate; N,N-dimethyl-formamide; 2.1: Schmidt Reaction;