(S)-3-{3-[2-(3-ethanesulfonyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one

Base Information

Chemical Name:(S)-3-{3-[2-(3-ethanesulfonyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one
CAS No.:1309614-19-4
Molecular Formula:C₂₃H₂₁NO₄S
Molecular Weight:407.49
Hs Code.:

Synonyms:(S)-3-{3-[2-(3-ethanesulfonyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one

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Chemical Property of (S)-3-{3-[2-(3-ethanesulfonyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one

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Technology Process of (S)-3-{3-[2-(3-ethanesulfonyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one

There total 2 articles about (S)-3-{3-[2-(3-ethanesulfonyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1309614-27-4
(S)-3-{3-[2-(3-ethanylsulfanyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one

: 1309614-19-4
(S)-3-{3-[2-(3-ethanesulfonyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1039/c1cc10551e

Reference yield:

: 1309614-26-3
C₂₂H₁₉NO₅S

: 1309614-19-4
(S)-3-{3-[2-(3-ethanesulfonyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

1.2: 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.67 h / 0 °C / Inert atmosphere

With 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c1cc10551e

Reference yield: 21.0%

: 1309614-19-4
(S)-3-{3-[2-(3-ethanesulfonyl-prop-1-ynyl)-phenyl]-prop-2-ynyl}-4-phenyl-oxazolidin-2-one

: (11R,11aR)-11-ethanesulfonyl-11a-phenyl-1,4,11,11a-tetrahydro-2-oxa-3a-azacyclopenta[b]anthracen-3-one

: 1309614-21-8
(11R,11aS)-11-ethanesulfonyl-11a-phenyl-1,4,11,11a-tetrahydro-2-oxa-3a-azacyclopenta[b]anthracen-3-one

: 1309614-23-0
(11S,11aS)-11-ethanesulfonyl-11a-phenyl-1,4,11,11a-tetrahydro-2-oxa-3a-azacyclopenta[b]anthracen-3-one

Guidance literature:: With mesoporous silica grafted with the tertiary amine group; In benzene; at 80 ℃; for 4h; optical yield given as %ee; Inert atmosphere;
DOI:10.1039/c1cc10551e