Technology Process of C22H34N2O3
There total 7 articles about C22H34N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H42N2O5;
With
trifluoroacetic acid;
In
dichloromethane;
at 25 ℃;
for 3h;
With
sodium hydroxide;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: caesium carbonate / dichloromethane / 30 h / 42 °C
2.1: magnesium / iodine / diethyl ether / 2.75 h / Inert atmosphere; Reflux
2.2: 2 h / -78 - 20 °C
2.3: 1 h / 0 - 20 °C
3.1: hydrogenchloride / 1,4-dioxane; methanol / 1.5 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane; N,N-dimethyl-formamide / 18 h / 20 °C
5.1: trifluoroacetic acid / dichloromethane / 3 h / 25 °C
With
hydrogenchloride; caesium carbonate; magnesium; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid;
iodine;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium / iodine / diethyl ether / 2.75 h / Inert atmosphere; Reflux
1.2: 2 h / -78 - 20 °C
1.3: 1 h / 0 - 20 °C
2.1: hydrogenchloride / 1,4-dioxane; methanol / 1.5 h / 20 °C
3.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane; N,N-dimethyl-formamide / 18 h / 20 °C
4.1: trifluoroacetic acid / dichloromethane / 3 h / 25 °C
With
hydrogenchloride; magnesium; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid;
iodine;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
