2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

Base Information

Chemical Name:2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester
CAS No.:271598-87-9
Molecular Formula:C₂₃H₂₇NO₂Si
Molecular Weight:377.558
Hs Code.:

Synonyms:2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

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Chemical Property of 2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

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Technology Process of 2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

There total 1 articles about 2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 69555-14-2
ethyl N-diphenylmethylene glycine

: 38002-45-8
3-bromo-1-(trimethylsilyl)-1-propyne

: 271598-87-9
2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

Guidance literature:: With potassium carbonate; In acetonitrile;
DOI:10.1039/a910217p

Reference yield: 77.0%

: 98-59-9
p-toluenesulfonyl chloride

: 271598-87-9
2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

: 271598-92-6
ethyl 2-{[(4-methylphenyl)sulfonyl]amino}pent-4-ynoate

: 271598-95-9
2-(toluene-4-sulfonylamino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

Guidance literature:: 2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester; With hydrogenchloride; water; In diethyl ether;

p-toluenesulfonyl chloride; With triethylamine; In dichloromethane; Further stages.;
DOI:10.1039/a910217p

Reference yield:

: 271598-87-9
2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

: 271599-12-3
ethyl N-[(4-methylphenyl)sulfonyl]-4-vinyl-1,2,3,6-tetrahydropyridine-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: HCl; H₂O / diethyl ether

1.2: 11 percent / Et₃N / CH₂Cl₂

2.1: 98 percent / K₂CO₃ / acetonitrile

3.1: 70 percent / (Cy₃P)Cl₂Ru=CHPh / toluene / 36 h / Heating

With hydrogenchloride; water; potassium carbonate; Grubbs catalyst first generation; In diethyl ether; toluene; acetonitrile; 1.1: Hydrolysis / 1.2: Tosylation / 2.1: Alkylation / 3.1: Cyclization;
DOI:10.1039/a910217p