pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate

Base Information

Chemical Name:pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate
CAS No.:1175707-06-8
Molecular Formula:C₁₆H₈Cl₅F₂O₅P
Molecular Weight:526.472
Hs Code.:

Synonyms:pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate

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Technology Process of pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate

There total 1 articles about pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1175707-04-6
pentachlorophenyl (E)-3-(4-(diethylphosphoryldifluoromethyl)phenyl)prop-2-enoate

: 1175707-06-8
pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate

Guidance literature:: With trimethylsilyl iodide; 2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol9012662

Reference yield: 64.0%

: 1175707-06-8
pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate

: 53064-79-2
iodomethyl pivaloate

: 1175707-09-1
pentachlorophenyl (E)-3-(4-(di(pivaloyloxymethyl)phosphoryldifluoromethyl)phenyl)prop-2-enoate

Guidance literature:: pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate; With sodium hydroxide; In water;

With silver nitrate; In water; at 4 ℃; for 2h; pH=10;

iodomethyl pivaloate; In toluene; at 20 ℃; for 24h;
DOI:10.1021/ol9012662

Reference yield:

: 1175707-06-8
pentachlorophenyl (E)-3-(4-(phosphoryldifluoromethyl)phenyl)prop-2-enoate

: C₂₅H₂₈N₅O₄Pol

: C₃₅H₃₅F₂N₅O₈PPol

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 3h; solid phase reaction;
DOI:10.1021/ol9012662