Acetic acid (1S,2R,3S,4R,5R)-4-acetoxy-2-((1R,4S,5R,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylamino)-6,8-dioxa-bicyclo[3.2.1]oct-3-yl ester

Base Information

• Chemical Name: Acetic acid (1S,2R,3S,4R,5R)-4-acetoxy-2-((1R,4S,5R,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylamino)-6,8-dioxa-bicyclo[3.2.1]oct-3-yl ester
• CAS No.: 132016-25-2
• Molecular Formula: C₂₅H₃₃NO₁₄
• Molecular Weight: 571.535

Synonyms:Acetic acid (1S,2R,3S,4R,5R)-4-acetoxy-2-((1R,4S,5R,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylamino)-6,8-dioxa-bicyclo[3.2.1]oct-3-yl ester

Chemical Property of Acetic acid (1S,2R,3S,4R,5R)-4-acetoxy-2-((1R,4S,5R,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylamino)-6,8-dioxa-bicyclo[3.2.1]oct-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Acetic acid (1S,2R,3S,4R,5R)-4-acetoxy-2-((1R,4S,5R,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylamino)-6,8-dioxa-bicyclo[3.2.1]oct-3-yl ester

There total 1 articles about Acetic acid (1S,2R,3S,4R,5R)-4-acetoxy-2-((1R,4S,5R,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylamino)-6,8-dioxa-bicyclo[3.2.1]oct-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-O-acetyl-1,6:3,4-dianhydro-β-D-galactopyranose (33159-54-5) + DL-4,7:5,6-di-O-isopropylidene-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenylamine (81692-19-5,86900-54-1,90025-02-8,109718-74-3,109718-75-4,132016-22-9) → Acetic acid (1S,2R,3S,4R,5R)-4-acetoxy-2-((1R,4S,5R,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylamino)-6,8-dioxa-bicyclo[3.2.1]oct-3-yl ester (132016-25-2) + Acetic acid (1S,2R,3S,4R,5R)-4-acetoxy-2-((1S,4R,5S,6S)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylamino)-6,8-dioxa-bicyclo[3.2.1]oct-3-yl ester (132016-24-1)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1039/c39900001387

Reference yield: 100.0%

Acetic acid (1S,2R,3S,4R,5R)-4-acetoxy-2-((1R,4S,5R,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylamino)-6,8-dioxa-bicyclo[3.2.1]oct-3-yl ester (132016-25-2) → (1R,2R,3S,6R)-6-((1S,2S,3S,4R,5R)-3,4-Dihydroxy-6,8-dioxa-bicyclo[3.2.1]oct-2-ylamino)-4-hydroxymethyl-cyclohex-4-ene-1,2,3-triol (132016-20-7)

Guidance literature:

With sodium methylate; In methanol;

DOI:10.1039/c39900001387

upstream raw materials:

2-O-acetyl-1,6:3,4-dianhydro-β-D-galactopyranose

DL-4,7:5,6-di-O-isopropylidene-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenylamine

Downstream raw materials:

(1R,2R,3S,6R)-6-((1S,2S,3S,4R,5R)-3,4-Dihydroxy-6,8-dioxa-bicyclo[3.2.1]oct-2-ylamino)-4-hydroxymethyl-cyclohex-4-ene-1,2,3-triol

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