C₅₃H₅₈Br₂O₆

Base Information

Chemical Name:C₅₃H₅₈Br₂O₆
CAS No.:474960-21-9
Molecular Formula:C₅₃H₅₈Br₂O₆
Molecular Weight:950.848
Hs Code.:

C<sub>53</sub>H<sub>58</sub>Br<sub>2</sub>O<sub>6</sub>

Synonyms:C₅₃H₅₈Br₂O₆

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Chemical Property of C₅₃H₅₈Br₂O₆

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Technology Process of C₅₃H₅₈Br₂O₆

There total 17 articles about C₅₃H₅₈Br₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: {3-(3-benzyloxy-5-decyloxy-benzyloxy)-5-[3-(3-bromo-benzyloxy)-5-(3-methyl-benzyloxy)-benzyloxy]-phenyl}-methanol

: 474960-21-9
C₅₃H₅₈Br₂O₆

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ol026746e

Reference yield:

: 99-10-5
3,5-Dihydroxybenzoic acid

: 474960-21-9
C₅₃H₅₈Br₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1: H₂SO₄ / Heating

2: lithium aluminium hydride

3: 82 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

4: 82 percent / NaBH₄ / Pd(PPh₃)4 / tetrahydrofuran / 24 h / 20 °C

5: 86 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

6: 82 percent / Ph₃P; NBS / tetrahydrofuran / 20 °C

7: 92 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

8: 87 percent / NaBH₄ / Pd(PPh₃)4 / tetrahydrofuran / 24 h / 20 °C

9: 89 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

10: 86 percent / Ph₃P; NBS / tetrahydrofuran / 20 °C

With sodium tetrahydroborate; N-Bromosuccinimide; lithium aluminium tetrahydride; 18-crown-6 ether; sulfuric acid; potassium carbonate; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; acetone;
DOI:10.1021/ol026746e

Reference yield:

: 4142-98-7
ethyl 3,5-dihydroxybenzoate

: 474960-21-9
C₅₃H₅₈Br₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1: lithium aluminium hydride

2: 82 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

3: 82 percent / NaBH₄ / Pd(PPh₃)4 / tetrahydrofuran / 24 h / 20 °C

4: 86 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

5: 82 percent / Ph₃P; NBS / tetrahydrofuran / 20 °C

6: 92 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

7: 87 percent / NaBH₄ / Pd(PPh₃)4 / tetrahydrofuran / 24 h / 20 °C

8: 89 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

9: 86 percent / Ph₃P; NBS / tetrahydrofuran / 20 °C

With sodium tetrahydroborate; N-Bromosuccinimide; lithium aluminium tetrahydride; 18-crown-6 ether; potassium carbonate; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; acetone;
DOI:10.1021/ol026746e