C₃₇H₄₄ClNO₈

Base Information

Chemical Name:C₃₇H₄₄ClNO₈
CAS No.:1261079-20-2
Molecular Formula:C₃₇H₄₄ClNO₈
Molecular Weight:666.211
Hs Code.:

C<sub>37</sub>H<sub>44</sub>ClNO<sub>8</sub>

Synonyms:C₃₇H₄₄ClNO₈

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Chemical Property of C₃₇H₄₄ClNO₈

Chemical Property:

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Technology Process of C₃₇H₄₄ClNO₈

There total 10 articles about C₃₇H₄₄ClNO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1261079-19-9
C₃₇H₄₅NO₇

: 1261079-15-5
C₃₇H₄₅NO₈

: 1261079-20-2
C₃₇H₄₄ClNO₈

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; water; In tetrahydrofuran; tert-butyl alcohol; at 10 - 25 ℃; for 48h;
DOI:10.1021/ol1027877

Reference yield:

: 2538-98-9
4-isopropyloxy-3-methoxybenzaldehyde

: 1261079-15-5
C₃₇H₄₅NO₈

: 1261079-20-2
C₃₇H₄₄ClNO₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: 6 h / 0 - 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane; water / 20 °C

3.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3.2: 8 h / 60 °C / Inert atmosphere

4.1: trichlorophosphate / 0.75 h / Cooling with ice

4.2: 0.25 h / 100 °C / Microwave irradiation; Sealed tube

4.3: Heating

5.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tetrahydrofuran; tert-butyl alcohol / 48 h / 10 - 25 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; potassium tert-butylate; water; trifluoroacetic acid; trichlorophosphate; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 1.2: Wittig reaction / 4.2: Vilsmeier-Haack formylation / 5.1: Lindgren oxidation;
DOI:10.1021/ol1027877

Reference yield:

: 34123-66-5
O-isopropylisovanillin

: 1261079-15-5
C₃₇H₄₅NO₈

: 1261079-20-2
C₃₇H₄₄ClNO₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonium acetate; acetic acid / 6 h / 100 °C

2.1: lithium borohydride; chloro-trimethyl-silane / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3.2: 8 h / 60 °C / Inert atmosphere

4.1: trichlorophosphate / 0.75 h / Cooling with ice

4.2: 0.25 h / 100 °C / Microwave irradiation; Sealed tube

4.3: Heating

5.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tetrahydrofuran; tert-butyl alcohol / 48 h / 10 - 25 °C

With sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; chloro-trimethyl-silane; 2-methyl-but-2-ene; ammonium acetate; water; acetic acid; trichlorophosphate; In tetrahydrofuran; tert-butyl alcohol; 4.2: Vilsmeier-Haack formylation / 5.1: Lindgren oxidation;
DOI:10.1021/ol1027877