(R)-2-acetamido-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester

Base Information

Chemical Name:(R)-2-acetamido-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester
CAS No.:1435781-02-4
Molecular Formula:C₅₀H₄₇NO₁₃S
Molecular Weight:901.988
Hs Code.:

Synonyms:(R)-2-acetamido-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester

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Chemical Property of (R)-2-acetamido-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester

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Technology Process of (R)-2-acetamido-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester

There total 7 articles about (R)-2-acetamido-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₈H₄₅NO₁₂S

: 108-24-7
acetic anhydride

: 1435781-02-4
(R)-2-acetamido-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1016/j.carres.2013.02.013

Reference yield:

: 1435780-53-2
allyl 2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

: 1435781-02-4
(R)-2-acetamido-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: tetraacetyl thioglucose / toluene / 33 h / 80 °C

2: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

3: pyridine / 12 h / 20 °C

With pyridine; tetraacetyl thioglucose; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1016/j.carres.2013.02.013

Reference yield:

: 1435780-98-5
(R)-2-(tert-butoxycarbonylamino)-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester

: 1435781-02-4
(R)-2-acetamido-3-(4-(α-D-tetra-O-benzoylglucosyloxy)-(E)-but-2-enylthio)propanoate benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

2: pyridine / 12 h / 20 °C

With pyridine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.carres.2013.02.013