Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Base Information

Chemical Name:Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside
CAS No.:116730-81-5
Molecular Formula:C₅₇H₅₆O₁₅
Molecular Weight:981.063
Hs Code.:

Synonyms:Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

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Chemical Property of Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

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Technology Process of Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

There total 4 articles about Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 34234-44-1
methyl 2,3,4-tri-O-benzoylglucopyranoside

: 4356-78-9
6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride

: 116730-81-5
Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

: 116730-77-9
methyl 6-O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; silver perchlorate; In diethyl ether; at -20 ℃; for 0.25h;
DOI:10.1016/0008-6215(88)84143-0

Reference yield:

: 34234-44-1
methyl 2,3,4-tri-O-benzoylglucopyranoside

: Acetic acid (2R,3R,4S,5R)-3,4,5-tris-benzyloxy-6-p-tolyltellanyl-tetrahydro-pyran-2-ylmethyl ester

: 116730-81-5
Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

: 116730-77-9
methyl 6-O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With lithium perchlorate; In acetonitrile; Yield given. Yields of byproduct given. Title compound not separated from byproducts; electrochemical oxidation;
DOI:10.1246/cl.1997.111

Reference yield:

: 4356-77-8
acetyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 116730-81-5
Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / HCl / diethyl ether / 48 h / Ambient temperature

2: silver perchlorate, 2,4,6-trimethyl pyridine / diethyl ether / 0.25 h / -20 °C

With 2,4,6-trimethyl-pyridine; hydrogenchloride; silver perchlorate; In diethyl ether;
DOI:10.1016/0008-6215(88)84143-0