C₁₄H₁₇FO₃

Base Information Edit

Chemical Name:C₁₄H₁₇FO₃
CAS No.:1338348-10-9
Molecular Formula:C₁₄H₁₇FO₃
Molecular Weight:252.286
Hs Code.:
Mol file:1338348-10-9.mol

C<sub>14</sub>H<sub>17</sub>FO<sub>3</sub>

Synonyms:C₁₄H₁₇FO₃

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Chemical Property of C₁₄H₁₇FO₃ Edit

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Technology Process of C₁₄H₁₇FO₃

There total 9 articles about C₁₄H₁₇FO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1307273-63-7
(-)-(6aR,8S,9R,9aR)-8-(benzyloxy)-9-fluoro-2,2,4,4-tetraisopropyl-7-methylenehexahydrocyclopenta[f][1,3,5,2,4]trioxadisilocine

: 1338348-10-9
C₁₄H₁₇FO₃

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2011.08.113

Reference yield:

: 1307273-58-0
(3aS,4S,6R,6aR)-6-(tert-butoxymethyl)-2,2-dimethyl-5-methylenetetrahydro-3aH-cyclopenta[d][1,3]-dioxol-4-ol

: 1338348-10-9
C₁₄H₁₇FO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran / 0.25 h / 20 °C

1.2: 3.5 h / 40 °C

2.1: hydrogenchloride; water / methanol / 3.5 h / Reflux

3.1: pyridine / -30 - 20 °C

4.1: trifluoromethylsulfonic anhydride; pyridine / dichloromethane / 0.33 h / -78 - 20 °C

4.2: 0.5 h / 50 °C

4.3: 3 h / 20 °C

5.1: diethylamino-sulfur trifluoride / dichloromethane / 0.33 h / 20 °C

6.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 20 °C

With pyridine; hydrogenchloride; trifluoromethylsulfonic anhydride; diethylamino-sulfur trifluoride; tetrabutyl ammonium fluoride; water; sodium hydride; acetic acid; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 1307273-61-5
(-)-(6aR,8S,9S,9aR)-8-(benzyloxy)-2,2,4,4-tetraisopropyl-7-methylenehexahydrocyclopenta[f][1,3,5,2,4]trioxadisilocin-9-ol

: 1338348-10-9
C₁₄H₁₇FO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoromethylsulfonic anhydride; pyridine / dichloromethane / 0.33 h / -78 - 20 °C

1.2: 0.5 h / 50 °C

1.3: 3 h / 20 °C

2.1: diethylamino-sulfur trifluoride / dichloromethane / 0.33 h / 20 °C

3.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 20 °C

With pyridine; trifluoromethylsulfonic anhydride; diethylamino-sulfur trifluoride; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; dichloromethane;