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Technology Process of C5H5Re(NO)CH(P(CH3)3)C6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5P(CH3)3PF6

C5H5Re(NO)CH(P(CH3)3)C6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5P(CH3)3PF6

Base Information
  • Chemical Name:C5H5Re(NO)CH(P(CH3)3)C6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5P(CH3)3PF6
  • CAS No.:82374-43-4
  • Molecular Formula:C33H35NOP2Re*F6P
  • Molecular Weight:854.766
  • Hs Code.:
C<sub>5</sub>H<sub>5</sub>Re(NO)CH(P(CH<sub>3</sub>)3)C<sub>6</sub>H<sub>5</sub>P(C<sub>6</sub>H<sub>5</sub>)3<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Re(C<sub>5</sub>H<sub>5</sub>)NOP(C<sub>6</sub>H<sub>5</sub>)3CHC<sub>6</sub>H<sub>5</sub>P(CH<sub>3</sub>)3PF<sub>6</sub>

Synonyms:C5H5Re(NO)CH(P(CH3)3)C6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5P(CH3)3PF6

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Chemical Property of C5H5Re(NO)CH(P(CH3)3)C6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5P(CH3)3PF6
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Technology Process of C5H5Re(NO)CH(P(CH3)3)C6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5P(CH3)3PF6

There total 1 articles about C5H5Re(NO)CH(P(CH3)3)C6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5P(CH3)3PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C<sub>5</sub>H<sub>5</sub>Re(NO)CHC<sub>6</sub>H<sub>5</sub>P(C<sub>6</sub>H<sub>5</sub>)3<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Re(C<sub>5</sub>H<sub>5</sub>)NOP(C<sub>6</sub>H<sub>5</sub>)3CHC<sub>6</sub>H<sub>5</sub>PF<sub>6</sub>
74540-78-6

C5H5Re(NO)CHC6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5PF6

trimethylphosphane
594-09-2

trimethylphosphane

C<sub>5</sub>H<sub>5</sub>Re(NO)CH(P(CH<sub>3</sub>)3)C<sub>6</sub>H<sub>5</sub>P(C<sub>6</sub>H<sub>5</sub>)3<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Re(C<sub>5</sub>H<sub>5</sub>)NOP(C<sub>6</sub>H<sub>5</sub>)3CHC<sub>6</sub>H<sub>5</sub>P(CH<sub>3</sub>)3PF<sub>6</sub>
82374-43-4

C5H5Re(NO)CH(P(CH3)3)C6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5P(CH3)3PF6

Guidance literature:
In not given; to -78°C soln. of Re-complex was added dropwise ligand, after 15min at -78°C mixt. was allowed to warm to room temp. under N2; solvent was removed in vac., residue was taken up in CH2Cl2, ether was diffused into soln. in a freezer;
DOI:10.1021/ja00382a021
upstream raw materials:

C5H5Re(NO)CHC6H5P(C6H5)3(1+)*PF6(1-)=Re(C5H5)NOP(C6H5)3CHC6H5PF6

trimethylphosphane

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