C₇₁H₁₃₆O₁₁Si₅

Base Information

Chemical Name:C₇₁H₁₃₆O₁₁Si₅
CAS No.:902132-48-3
Molecular Formula:C₇₁H₁₃₆O₁₁Si₅
Molecular Weight:1306.28
Hs Code.:

C<sub>71</sub>H<sub>136</sub>O<sub>11</sub>Si<sub>5</sub>

Synonyms:C₇₁H₁₃₆O₁₁Si₅

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Chemical Property of C₇₁H₁₃₆O₁₁Si₅

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Technology Process of C₇₁H₁₃₆O₁₁Si₅

There total 33 articles about C₇₁H₁₃₆O₁₁Si₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 902132-46-1
C₇₄H₁₄₄O₁₁Si₆

: 902132-48-3
C₇₁H₁₃₆O₁₁Si₅

Guidance literature:: With potassium carbonate; In methanol; diethyl ether; at 25 ℃; for 4h;
DOI:10.1039/b602020h

Reference yield:

: 902132-11-0
(3R,4S)-3-(4-methoxybenzyloxy)-4-methyl-5-hexenal

: 902132-48-3
C₇₁H₁₃₆O₁₁Si₅

Guidance literature:: Multi-step reaction with 13 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C

1.2: tetrahydrofuran; hexane / 2 h / -78 - 0 °C

2.1: 93 percent / imidazole; 4-DMAP / CH₂Cl₂ / 2 h / 20 °C

3.1: O₃ / CH₂Cl₂ / -78 °C

3.2: 98 percent / PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

4.1: 98 percent / benzene / 16 h / 70 °C

5.1: 99 percent / DIBAL-H / tetrahydrofuran / 0.5 h / 0 °C

6.1: Et₃N / tetrahydrofuran / 1 h / 0 °C

7.1: 2.004 g / LiBr / tetrahydrofuran / 0.75 h / 25 °C

8.1: LDA / tetrahydrofuran / 1.5 h / -78 °C

8.2: 84 percent / tetrahydrofuran / 1 h / -78 °C

9.1: LDA / tetrahydrofuran / 2 h / -78 °C

9.2: tetrahydrofuran / 4 h / -78 °C

10.1: 1.811 g / aq. (CO₂H)2 / diethyl ether / 40 h / 25 °C

11.1: 64 percent / TsOH*H₂O / methanol; CH₂Cl₂ / 20 h / 25 °C

12.1: 54 percent / 2,6-lutidine / CH₂Cl₂ / 1.5 h / 0 °C

13.1: 84 percent / K₂CO₃ / methanol; diethyl ether / 4 h / 25 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; n-butyllithium; oxalic acid; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; ozone; triethylamine; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; benzene; 4.1: Wittig reaction;
DOI:10.1039/b602020h

Reference yield:

: 902131-93-5
C₃₉H₇₇IO₅Si₃

: 902132-48-3
C₇₁H₁₃₆O₁₁Si₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: 90 percent / DDQ; aq. pH 7.0 buffer / CH₂Cl₂ / 1 h / 25 °C

2.1: 65 percent / pyridine; 4-DMAP / CH₂Cl₂ / 22 h / 0 - 25 °C

3.1: LDA / tetrahydrofuran / 2 h / -78 °C

3.2: tetrahydrofuran / 4 h / -78 °C

4.1: 1.811 g / aq. (CO₂H)2 / diethyl ether / 40 h / 25 °C

5.1: 64 percent / TsOH*H₂O / methanol; CH₂Cl₂ / 20 h / 25 °C

6.1: 54 percent / 2,6-lutidine / CH₂Cl₂ / 1.5 h / 0 °C

7.1: 84 percent / K₂CO₃ / methanol; diethyl ether / 4 h / 25 °C

With pyridine; 2,6-dimethylpyridine; dmap; oxalic acid; potassium carbonate; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1039/b602020h