2,4,6-trifluorobenzimidamide acetate

Base Information

Chemical Name:2,4,6-trifluorobenzimidamide acetate
CAS No.:1005460-16-1
Molecular Formula:C₂H₄O₂*C₇H₅F₃N₂
Molecular Weight:234.178
Hs Code.:

Synonyms:2,4,6-trifluorobenzimidamide acetate

Suppliers and Price of 2,4,6-trifluorobenzimidamide acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,4,6-trifluorobenzimidamide acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,4,6-trifluorobenzimidamide acetate

There total 4 articles about 2,4,6-trifluorobenzimidamide acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207204-82-7
2,4,6-trifluoro-N'-hydroxybenzimidamide

: 108-24-7
acetic anhydride

: 1005460-16-1
2,4,6-trifluorobenzimidamide acetate

Guidance literature:: 2,4,6-trifluoro-N'-hydroxybenzimidamide; acetic anhydride; With acetic acid; at 20 ℃; for 0.5h;

With 5% Pd(II)/C(eggshell); hydrogen; for 2.5h; under 1520.1 Torr;
DOI:10.1016/j.bmcl.2009.10.119

Reference yield:

: 96606-37-0,103498-69-7
2,4,6-trifluorobenzonitrile

: 1005460-16-1
2,4,6-trifluorobenzimidamide acetate

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; potassium carbonate / dimethyl sulfoxide / 20 °C

2: acetic acid / 0.5 h / 20 °C

3: 5%-palladium/activated carbon; hydrogen / 2.5 h / 1520.1 Torr

With 5%-palladium/activated carbon; hydroxylamine hydrochloride; hydrogen; potassium carbonate; acetic acid; In dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2014.07.032